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A8L1471 Ekiiiiiiiiiiiiili General: Heavy Metals ASSOCIATES BSK Associates Laboratory Fresno Metals Quality Control Report Spike Source %REC RPD Date Analyte Result RL Units Level Result %REC Limits RPID Limit Analyzed Qual EPA 6020-Quality Control Batch:A818732 Prepared: 12/15/2018 Prep Method:EPA 3010A for TCLP(EPA 1311) Analyst: MAS Matrix Spike Dup(A818732-MSD1),Source:A81-1471-01 Barium,TCLP 9.6 0.20 mg/L 8.0 2.2 93 75-125 0 20 12/17/18 Beryllium,TCLP 7.6 0.050 mg/L 8.0 ND 94 75-125 4 20 12/17/18 Cadmium,TCLP 7.4 0.050 mg/L 8.0 ND 92 75-125 4 20 12/17/18 Chromium,TCLP 8.0 0.40 mg/L 8.0 ND 100 75-125 2 20 12/17/18 Cobalt,TCLP 7.9 0.40 mg/L 8.0 ND 98 75-125 4 20 12/17/18 Copper,TCLP 7.7 0.20 mg/L 8.0 ND 96 75-125 3 20 12/17/18 Lead,TCLP 7.7 0.20 mg/L 8.0 ND 96 75-125 2 20 12/17/18 Molybdenum,TCLP 8.4 0.40 mg/L 8.0 ND 105 75-125 3 20 12/17/18 Nickel,TCLP 8.0 0.40 mg/L 8.0 ND 100 75-125 2 20 12/17/18 Selenium,TCLP 7.3 0.080 mg/L 8.0 ND 91 75-125 2 20 12/17/18 Silver,TCLP 3.7 0.40 mg/L 4.0 ND 93 75-125 3 20 12/17/18 Thallium,TCLP 7.7 0.50 mg/L 8.0 ND 96 75-125 2 20 12/17/18 Vanadium,TCLP 8.2 0.40 mg/L 8.0 ND 103 75-125 3 20 12/17/18 Zinc,TCLP 7.4 2.0 mg/L 8.0 ND 92 75-125 4 20 12/17/18 EPA 6020-Quality Control Batch:A818733 Prepared: 12/15/2018 Prep Method:EPA 3010A for STLC/DISTLC Analyst: MAS Blank(A818733-BLK1) Antimony,WET ND 0.50 mg/L 12/17/18 Arsenic,WET ND 0.10 mg/L 12/17/18 Barium,WET ND 0.25 mg/L 12/17/18 Beryllium,WET ND 0.050 mg/L 12/17/18 Cadmium,WET ND 0.050 mg/L 12/17/18 Chromium,WET ND 0.50 mg/L 12/17/18 Cobalt,WET ND 2.5 mg/L 12/17/18 Copper,WET ND 0.50 mg/L 12/17/18 Lead,WET ND 0.25 mg/L 12/17/18 Molybdenum,WET ND 0.50 mg/L 12/17/18 Nickel,WET ND 0.50 mg/L 12/17/18 Selenium,WET ND 0.10 mg/L 12/17/18 Silver,WET ND 0.50 mg/L 12/17/18 Thallium,WET ND 0.50 mg/L 12/17/18 Vanadium,WET ND 0.50 mg/L 12/17/18 Zinc,WET ND 2.5 mg/L 12/17/18 Blank Spike(A818733-BS1) Antimony,WET 8.4 0.50 mg/L 8.0 ND 105 75-125 12/17/18 Arsenic,WET 8.3 0.10 mg/L 8.0 ND 104 75-125 12/17/18 Barium,WET 7.8 0.25 mg/L 8.0 ND 98 75-125 12/17/18 Beryllium,WET 7.7 0.050 mg/L 8.0 ND 97 75-125 12/17/18 Cadmium,WET 7.6 0.050 mg/L 8.0 ND 96 75-125 12/17/18 Chromium,WET 8.3 0.50 mg/L 8.0 ND 104 75-125 12/17/18 Cobalt,WET 8.1 2.5 mg/L 8.0 ND 101 75-125 12/17/18 Copper,WET 7.8 0.50 mg/L 8.0 ND 97 75-125 12/17/18 The results in this report apply to the samples analyzed in A811471 FINAL 12272018 1717 accordance with the chain of custody document. This analytical report must be reproduced in its entirety. www.BSKAssociates.com Page 9 of 18