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1 <br /> MLNIMUM VERIFICATION LABORATORY ANALYSIS <br />' TANK TANK TPH-0 TPH-D BTX & E CL HC TOTAL EDB METALS PCB <br /> # CONTENTS 8015 8015 8020 8010 LEAD )CAP/ 8270 <br /> 8260 8260 8260 8240 7420 8240 AES or 8080 <br /> 7421 AA <br />' O ) LEADED X X <br /> GAS X X <br /> 5 X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> PROD OIL X X <br />' CHLOR <br /> SOLVENTS X X <br />' NONCHLORTS <br /> SOLVENX X X <br />' WASTE\ X X <br /> USED OIL X X X X <br /> All analyses methods are designated EPA methods described in EPA SW 846, Third Edition Those methods not found <br /> bIn SW 846, are specifically noted below Refer to the 'SWRCB LUPI' Field Manual% Appendix A-20, Table 3-5 for <br /> defeclion limits of motor vehicle fuels (gasoline and diesel) Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> initial Evaluation and Investigation of USTs" for the waste and motor oil detection limits <br /> Detection Limits that remain below the MCI., STLC or Allowable Limit or the contaminant In question will be accepted, <br />' however laboratory shall utilize the most conservative method. <br />' <br /> LABORATORY ANALYSES TERMINOLOGY 5030 8015 mod or GGMS 8260 <br /> 3TPH_G Total Petroleum Hydrocarbon, Gasoline, GCJFID ( ) <br /> 50), 8(115 mod or GC/MS 8260 <br /> TPII-D Total Petroleum Hydrocarbon, Diesel, GCIM (35 <br /> B rX & E Benzene, Toluene, Xylene & Ethyl Benzene, GC/PlD 8020 or GGMS 8260 <br />' CL HC Chlorinated Hydrocarbon, GC1iSD 8010, GC7MS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibrom)de (DHS-AB 1803), GCIMS 8240 (DHS-LUFT) <br /> GC FID Gas Chromatography, Flame Ionization Detection <br /> ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000 Metals: Cadmium, Chromium III and YI, Lead, Zinc and Nickel. <br /> PCB Polychlorinated Blphenyls, GOMS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonlcation sample preparation, attraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes, To avoid false positive detection of benzene, benzene-free solvents are to be used Fused capillary columns are <br /> preferred to packed columns, a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better Samples exhibiting any level of heavy metal <br /> contamination may require further analysis PHS-EHD recommends holding these samples until disposal is indicated. <br /> EH 23 048 (Revised 7/10192) Page 8 <br /> 1La.-h,� d4 k n <br /> -fxrl K rn sr� G <br />