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' 2852 Alton Ave Irvine CA 92606 (949)261 1022 FAX(949)261 1228 <br /> Del Mar Anal Teal 1014E Cooley it -12 A Colton CA 92324 (909)379 1844 FAX(909)370-'f046 <br /> 7277 Hayvenhurst Suite B-12 Van Nuys GA 91406 (81 B)779 1844 FAX(618)779-1843 <br /> 9484 Chesapeake Or Suite 805 San Diego CA 92123 (858)505-9596 FAX(858)505 9689 <br /> 9830 South 51st St Suite B 120 Phoenix AZ 85044 (460)785-0043 FAX(480)785 0851 <br /> AM Environmental-San Diego Client Pralect lD EZ Serve#100966/Stockton,CA <br /> 9620 Cheaspeake Drive,Suite 203 43 25827 0026 Sampled 11/06/01 <br /> San Diego,CA 92123 Report Number CKKO104 Received 11/09/01 <br /> Attention Mike Davis <br /> METHOD BLANK/QC DATA <br /> , , - <br /> OXYGENATES by GC/M[S (EPA 8260B) <br /> Reporting Spike Source %REC RPD Data <br /> Analyte Result Limit Units Leve! Result %REC Limits RPD Limit Qualifiers <br /> batch. CIK1412 Extracted: 11/14/01 <br /> Blank Analyzed 11/14/01 (OK1412-BLK1) <br /> i-isopropyl Ether(D1PE) ND 20 ug/l <br /> thyl tert-Butyl Ether(ETBE) ND 20 ugll <br /> Methyl-tert-butyl Ether(MTBE) ND 10 ug/l <br /> tert-Amyl Methyl Ether(TAME) ND 20 ugA <br /> trt-Butanol(TBA) ND 25 ug/l <br /> urrogate Dibromofluoromethane 295 ug/l 250 118 80-140 <br /> Surrogate Toluene-d8 277 ug/1 250 111 80-135 <br /> 4-Bromofluorobenzene 283 ugA 250 113 80-145 <br /> tuWate <br /> nalyzed: 11/14/01 (C1K1412-BS1) <br /> Di-isopropyl Ether(DIPE) 220 20 ug/l 250 880 65-155 <br /> Ihyl tert-Butyl Ether(ETBE) 250 20 ug/l 250 100 55-145 <br /> ethyl-tert-butyl Ether(MTBE) 237 10 ug/l 250 948 65-135 <br /> tert-Amyl Methyl Ether(TAME) 232 20 ug/1 250 928 65-140 <br /> r#-Butanol(TBA) 134 25 ug/l 125 107 60-150 <br /> urrogate Dibromofluoromethane 300 ug/1 250 120 80-140 <br /> urrogate Toluene-d8 278 ug/7 250 111 80-135 <br /> Surrogate 4-Bromofluorobenzene 306 ug/1 250 122 80-145 <br /> katrix Spike Analyzed: 11/15/01 (ClK1412-MS1) Source: CKKO100-02 <br /> '-Lsopropyl Ether(DiPE) 220 20 ugfl 250 ND 880 65-160 <br /> fe"rt-Amyl <br /> hyl tert-Butyl Ether(ETBE) 249 20 ug/1 250 ND 996 50-145 <br /> ethyl-tert-butyl Ether(MTBE) 238 10 ugA 250 ND 952 60-135 <br /> Methyl Ether(TAME) 235 20 ug/l 250 ND 940 60-140 <br /> tent-Butanol(TBA) 132 25 ug/l 125 ND 106 60-160 <br /> turrogate Dibromofluoromethane 303 ug/l 250 121 80-140 <br /> urrogate Toluene-d8 280 ug17 250 112 80-135 <br /> Surrogate 4-Bromofluorobenzene 297 U8,4 250 119 80-145 <br /> el Mar Analytical, Colton <br /> Tifton J Kiser <br /> Protect Manager <br /> The results pertain only to the samples tested in the laboratory This report shall not be reproduced <br /> except m full without written permission from Del Mar Analytical CKKO104 <Page 19 of 24a <br />