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' 2852 Alcon Ave trwne CA 92606 (949)261 1022 FAX(949)261 1228 <br /> •cal 1014 E Cooley Dr Suite A Calton CA 92324 (909)370.4667 FAX(909)370 1046 <br /> 7277 Hayvenhumt Suite 8-12 Ven Nuys CA 91406 (818)779-1844 FAX(818)779 1843 <br /> Del MarAnalo <br /> 9484 Chesapeake Dr Suite 805 San Diego CA 92123 (858)505-9596 FAX(858)505 9689 <br />' 9830 South 51st St Suite B 120 Phoenix AZ 65044 (480)7850043 FAX(480)785 0851 <br /> A I U Environmental-San Diego Client Project ID EZ Serve#100966/Stockton,CA <br /> 9620 Cheaspeake Drive,Suite 203 43 25827 0026 Sampled 11/06/01 <br /> San Diego,CA 92123 Report Number CKKO104 Received 11/09/01 <br /> Attention Mike Davis <br /> F METHOD BLANK/QC DATA <br /> OXYGENATES by GUMS (EPA 8260B) <br /> 1 Reporting Sptke Source %REC RPD Data <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Qualifiers <br /> Batch CIK1412 Extracted: 11/14/01 <br /> Matrix Spike Dup Analyzed- 11/15/01 (CIK1412-MSD1) Source CKKO100-02 <br /> Iti-isopropyl Ether(DIPE) 230 20 ug/I 250 ND 920 65-160 444 20 <br /> hyl tert-Butyl Ether(ETBE) 258 20 ug/1 250 ND 103 50-145 355 20 <br /> ethyl-tert-butyl Ether(MTBE) 244 10 ug/1 250 ND 976 60-135 249 20 <br /> tert-Amyl Methyl Ether(TAME) 240 20 ug/1 250 ND 960 60-140 211 20 <br /> lrt-Butanol(TBA) 129 25 ug/l 125 ND 103 60-160 230 35 <br /> urrogate Dtbromofluoromethane 300 ugR 250 120 80-140 <br /> Surrogate Toluene-d8 278 ugR 250 HI 80-135 <br /> tWOK1505 <br /> te 4-Bromofluorobenzene 295 ugll 250 118 80-145 <br /> ,Extracted:311151 1 <br /> lank Analyzed: 11/15/01 (ClK1505-BLK1) <br /> i-isopropyl Ether(DTPE) ND 20 ug/l <br /> Ethyl tert-Butyl Ether(ETBE) ND 20 ug/1 <br /> ethyl-tert-butyl Ether(MTBE) ND 10 ug/1 <br /> rt-Amyl Methyl Ether(TAME) ND 20 ug/l <br /> rt-Butanol(TBA) ND 25 ug/1 <br /> Surrogate Dtbromofluoromethane 253 ugR 250 101 80-140 <br /> Irrogate Toluene-d8 236 ugR 250 944 80-135 <br /> rrogate 4-Bromofluorobenzene 211 ug/7 250 844 80-145 <br /> CS Analyzed: 11/15/01 (C1K1505-BS1) <br /> i-isopropyl Ether(DIPE) 243 20 ug/l 250 972 65-155 <br /> thyl tert-Butyl Ether(ETBE) 219 20 ug/1 250 876 55-145 <br /> Methyl-tert-butyl Ether(MTBE) 206 10 ug/l 250 824 65-135 <br /> Irt-Amyl Methyl Ether(TAME) 211 20 ug/1 250 844 65-140 <br /> rt-Butanol.(TBA) 1.31 25 ug/1 125 105 60-150 <br /> Surrogate Dtbromofluoromethane 228 ug/7 250 912 80-140 <br /> frrogate Toluene-d8 261 ugR 250 104 80-135 <br /> rrogate 4-Bromofluorobenzene 206 ug/7 250 824 80-145 <br /> 1 <br /> PeRar <br /> Analytical, Colton <br /> lifton J Kiser <br /> Project Manager <br /> The results pertain only to the samples tested in the laboratory This report shall not be reproduced <br /> except in full,without written permission from Del Mar Analytical CKKO104 <Page 20 of 24> <br />