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MAT= SPIKE SAMPLE EVALUATION REPORT TOTAL, Metals Client Lot #. .. : G3C270312 Matrix.. . .. . . ..: SOLID Date Sampled. _ .: 03/27/03 Date Received..: 03/27/03 PERCENT RECOVERY RPD PREPARATION- WORK PARAMETER RECOVERY LIMITS RPD LIMITS METHOD ANALYSIS DATE ORDER # MS Lot-Sample #: E3C280158-001 Prep Batch #.-.: 3090265 Antimony 37 N (80 - 103) SW846 6020 03/31-04/04/03 PKXR31DC 37 N (80 - 103) 0.44 (0-20) SW846 6020 03/31-04/04/03 FKXR31DD Dilution Factor: 1 Arsenic 86 (80 - 102) SW846 6020 03/31-04/04/03 FKXR31CG 81 (80 - 102) 4.2 (0-20) SW846 6020 03/31-04/04/03 FKXR31CH Dilution Factor: 1 Barium 268 N (85 - 109) SW846 6020 03/31-04/04/03 FKKR3ICJ 168 N (85 - 109) 19 (0-20) SW846 6020 03/31-04/04/03 FMM3ICK Dilution Factor: 1 Beryllium 84 (77 - 100) SW846 6020 03/31-04/04/03 FKKR3ICL 84 (77 - 100) 1.0 (0-20) SW846 6020 03/31-04/04/03 FK=lCM Dilution Factor: 1 Cadmium 89 (81 - 103) SW846 6020 03/31-04/04/03 FKKR31CQ 85 (81 - 103) 2.9 (0-20) SW846 6020 03/31-04/04/03 FKKR31CR Dilution Factor: 1 Chromium 134 N (82 - 114) SW846 6020 03/31-04/04/03 FKXR3ICX 113 (82 - 114) 9.5 (0-20) SW846 6020 03/31-04/04/03 FKKR31C0 Dilution Factor: 1 Cobalt 103 (83 - 119) SW846 6020 03/31-04/04/03 FKXR3ICV 90 (83 - 119) 9.2 (0-20) SW846 6020 03/31-04/04/03 FKKR31CW Dilution Factor: i Copper 95 (86 - 110) SW846 6020 03/31-04/04/03 FKXR3IDT 81 N (86 - 110) 9.1 (0-20) SW846 6020 03/31-04/04/03 FKXR31DU Dilution Factor: 1 Lead 103 (80 - 118) SW846 6020 03/31-04/04/03 FKXR31C9 95 (80 - 118) 5.7 (0-20) SW846 6020 03/31-04/04/03 FKXR31DA Dilution Factor: 1 Molybdenum 87 (86 - 110) SW846 6020 03/31-04/04/03 FKXR31C5 83 N (86 - 110) 3.4 (0-20) SW846 6020 03/31-04/04/03 FKXR31C6 Dilution Factor: 1 (Continued on next page)