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t+ATR.:EX SPIES SAMPLE DATA REPORT TOTAL Metals Client Lot <_ . _ : G3C270312 Matrix- . .. . ... SOLID Date Sampled_: 03/27/03 Date Received_ _: 03/27/03 SAMPLE SPIKE MEASRD PERCNT PREPARATION- WORK PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER MS Lot-Sample #: E3C280158-001 Prep Batch t_ _.: 3090265 Antimony 0.11 4 .76 1.89 N mg/kg 37 SW846 6020 03/31-04/04/03 FKXR31DC 0.11 4.81 1.90 N mg/kg 37 0.44 SW846 6020 03/31-04/04/03 FKM31DD Dilution Factor: 1 Arsenic 3.1 19.0 19.5 mg/kg 86 SW846 6020 03/31-04/04/03 FKXR31CG 3 .1 19.2 18 .7 mg/kg 81 4.2 SW846 6020 03/31-04/04/03 FRXR31CH Dilution Factor: 1 Barium 57.4 19.0 108 N mg/kg 268 SW846 6020 03/31-04/04/03 FKXR31CJ 57.4 19.2 89.7 N mg/kg 168 19 SW846 6020 03/31-04/04/03 FKXR31CK Dilution Factor: 1 Beryllium 0.58 19.0 16.6 mg/kg 84 SW846 6020 03/31-04/04/03 FKXR3" 0.58 19.2 16.8 mg/kg 84 1.0 SW846 6020 03/31-04/04/03 FKXR3. Dilution Factor: i Cadmium 0.050 19.0 17.0 mg/kg 89 SW846 6020 03/31-04/04/03 FKXR31CQ 0.050 19.2 16.6 mg/kg 85 2.9 SW846 6020 03/31-04/04/03 MR31CR Dilution Factor: 1 Chromium 17.2 19.0 42.8 N mg/kg 134 SW846 6020 03/31-04/04/03 PKKR31CX 17.2 19.2 38.9 mg/kg 113 9.5 SW846 6020 03/31-04/04/03 FKXR31CO Dilution Factor: i Cobalt 6.5 19.0 26.0 mg/kg 103 SW846 6020 03/31-04/04/03 FKXR31CV 6.5 19.2 23 .7 mg/kg 90 9.2 SW846 6020 03/31-04/04/03 FKM31CW Dilution Factor: i Copper 10.3 19.0 28.4 mg/kg 95 SW846 6020 03/31-04/04/03 FKXR31DT 10.3 19.2 25.9 N mg/kg 81 9.1 SW846 6020 03/31-04/04/03 F=IDU Dilution Factor: 1 (Continued on next page)