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Q U A L I T Y C O N T R O L R E 5 U L T 5 <br /> Job Number 992710 Report Date 01/06/2000 <br /> CUSTOMER 1T Group PROJECT Southland Martinez ATTN Rhonda Teicheira <br /> QC Type Description Reag Cade Lab ID Dilution Factor Date Ttme <br /> M5 Matrix Spike 09120705 992648-1 12/27/1999 0730 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> ert-Butyl Alcohol (TBA) 1233 46 1000 000000 178 95 105 5 48-194 <br /> i isopropyl Ether 57 90 50 000000 0 115 8 53-149 <br /> Ethyl tert-Butyl Ether (ETBE) 55 97 50 000000 0 111 9 53-148 <br /> ert-Amyl Methyl Ether 57 01 50 000000 0 114 D 49-158 <br /> ethyl-t-Butyl Ether (MTBE) 120 92 100 000000 11 55 109 4 44-190 <br /> 1,2-Dichloroethane 10 64 10 000000 0 106 4 70-130 <br /> 1,2-Dibromoethane (EDB) 11 95 10 000000 0 119 5 70-130 <br /> MSD Matrix Spike Duplicate 09120705 992648-1 12/27/1999 0803 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> r 1306 00 1233 46 1000 000000 178 95 112 7 48-194 <br /> ert-Butyl Alcohol (TBA) 6 21 <br /> Di-Isopropyl Ether 58 24 57 90 50 000000 0 116 5 53-149 <br /> 1 15 <br /> tert-Butyl Ether (ETBE) 54 85 55 97 50 000000 0 109 7 53-148 <br /> 2 28 <br /> Pert-AmyL Methyl Esther 54 54 57 01 50 000000 0 109 1 49-156 <br /> 4 48 <br /> ethyl-t-Butyl Ether (MTBE) 121 52 12D 92 100 000000 11 55 110 0 44-190 <br /> r <br /> 0 21 <br /> ,2-Dichloroethane 10 27 10 64 10 000000 0 102 7 70-130 <br /> 4 30 <br /> 1,2-Dibromoethane (EDB) 11 27 11 95 10 000000 0 112 7 70-130 <br /> 1 6 30 <br /> LCS Laboratory Control Sample09123101 12/31/1999 0204 <br /> Parameter/Test Description 4C Result QC Result True Value Orig Value Calc Result " Limits F <br /> tert-Butyl Alcohol (TBA) 1004 81 1000 000000 100 5 37-175 <br /> i-isopropyl Ether 60 48 50 000000 121 0 60-138 <br /> thyL tert-Butyl Ether (ETBE) 51 79 50 000000 103 6 51-143 <br /> 4 <br /> ert-AmyL Methyl Ether 54 49 50 000000 109 0 64-137 <br /> Methyl t-ButyL Ether (MTBE) 102 52 100 000000 102 5 33-169 <br /> 1,2-Dichloroethane 10 23 10 000000 102 3 70-130 <br /> ,2-Dibromoethane (EDB) 11 49 10 000000 114 9 70-130 <br /> E <br /> Method Blank 12/31/2099 0236 <br /> Parameter/Test Description QC Result QC Result True Value Orig Value Calc Result * Limits F <br /> tert-Butyl Alcohol (FBA) 0 <br /> Di-Isopropyl Ether 1 32 <br /> Wthyl <br /> tert-Butyl Ether (ETBE) 0 <br /> ert Amyl Methyl Ether 0 <br /> L-t-Butyl Ether (MTBE) 0 <br /> i ch loroetharie 0 <br /> ibromoethane (EDB) 0 <br /> Page 12 * X=X REC, R=RPD, A=A65 Diff D=1G Diff <br />