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S U R R O G A T E R E C O V E R I E S R E P O R T Job Number 992710 Report Date 01/06/2000 CUSTOMER IT Group PRDJECT• Southland - Martinez ATTN Rhonda Teicheira Method Volatile organics by GC/MS Batch 10423 Method Code 8260OX Analyst am Surrogate Units DlbromofLuoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 992556-6 Solid 1 23 48 25 000 93 9 60-160 12/07/1999 1442 992556-6 Solid MS 23 57 25 000 94 3 60-160 12/07/1999 1705 992556-6 Solid MSD 24 61 25 000 98 4 60-160 12/07/1999 1740 992648-1 Solid 1 26 37 25 000 105 5 60-160 12/27/1999 0338 992648-1 Solid MS 26 11 25 000 104 4 60-160 12/27/1999 0730 992648-1 Solid MSD 25 45 25 000 101 8 60-160 12/27/1949 0803 LCS 1 25 59 25 000 102 4 57-162 12/31/1999 0204 r 992707-3 Solid 1 27 75 25 000 111 0 60-160 12/31/1999 0309 992707-4 Solid 1 26 82 25 000 107 3 60-160 12/31/1999 0342 992707-5 Solid 1 25 95 25 000 103 8 60-160 12/31/1999 0414 Y&710-2 Solid 1 26 99 25 000 108 0 60-160 12/31/1999 0447 1"` 10-3 Solid 1 25 88 25 000 103 5 60-160 12/31/1999 0519 10-4 Solid 1 26 18 25 000 104 7 60-16D 12/31/1999 0552 992710-7 Solid 1 25.77 25 000 103 1 60 160 12/31/1999 0624 992710-8 Solid 1 26 14 25 000 104 6 60-160 12/31/1999 0657 992710-9 Solid 1 25 43 25 000 101 7 60-160 12/31/1999 0729 ! 992709-3 Solid 1 27 25 25 000 109 0 60-160 12/31/1999 0802 i 992709-4 Solid 1 26 46 25 000 105 8 60-160 12/31/1999 0834 992709-7 Solid 1 26 78 25 000 107 1 60-160 12/31/1994 0907 MB 1 25 64 25 000 102 6 57-162 12/31/2099 0236 Method Volatile Organics -Aromatics Batch 10442 Method Code 8020BX Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L Lab ID Matrix QCType Dilution Result True Value Percent Recovery Limits Flag Date Time CV 1 44 53 50 0000 89 1 74-147 01/05/2000 1953 MB 1 42 59 50 0000 85 2 64-147 01/05/2000 2019 992712-1 Solid 1 43 64 50 0000 87 3 64-147 01/05/2000 2045 992712-3 Solid 1 43 08 50 0000 86 2 64-147 01/05/2000 2111 992693-9 Solid 1 40 86 50 0000 81 7 64-147 01/05/2000 2137 992693-3 Solid 1000 70 61 50 0000 141 2 64-147 01/05/2000 2203 992709-7 Solid 1 42 63 50 0000 85 3 64-147 01/05/2000 2230 992705-4 Solid 5 82 80 50 0000 165.6 64-147 X 01/05/2000 2256 992711-1 Liquids 5 42 22 50 0000 84 4 64-147 01/05/2000 2323 992707-4 Solid 1 41 24 50 0000 82 5 64-147 01/05/2000 2349 992707-5 Solid 1 42 44 50 0000 84.9 64-147 01/06/2000 0015 710-2 Solid 1 43 48 50 0000 87.0 64-147 01/06/2000 0041 CV 1 43 99 50 0000 88 0 64-147 01/06/2000 0134 CV 1 43 34 50 0000 86 7 64-147 01/06/2000 0227 ' 992710-3 Solid 1 43 16 50 0000 86 3 64-147 01/06/2000 0253 Page 13