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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: #4701065871 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/22/17 09:13 <br /> Bottom Ash Weekly Composite <br /> 1702046-02(Soil) <br /> Reporting Date Date <br /> Analyte Result Limit Units Batch Prepared Analyzed Method Notes <br /> Wet Chemistry <br /> pH 12.388 0.10000 pH Units A[B0117 02/14/17 02/14/17 EPA 9040B <br /> Total Recoverable Metals <br /> Arsenic 4.8 1.0 mg/kg A[B0097 02/10/17 02/10/17 EPA 6010B <br /> Lead 3.9 1.0 " <br /> STLC Analysis <br /> Arsenic 0.4 0.2 mg/L A[B0136 02/14/17 02/15/17 EPA 6010B <br /> Lead ND 0.2 " " " " <br /> 11 <br /> EXcelchern Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> y custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 3 of <br />