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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: #4701065871 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/22/17 09:13 <br /> Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A[B0117-EPA 9040B <br /> Duplicate(A[B0117-DUPl) Source:1702067-01 Prepared&Analyzed:02/14/17 <br /> pH 12.349 0.10000 pH Units 12.433 0.678 20 <br /> EXcelchern Environn-iental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> y custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 4of7 <br />