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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: #4701065871 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/22/17 09:13 <br /> Sample integrity WORK ORDER 1702.046 <br /> Date Deceived- 02JOS12017 <br /> ^+ettin[s 1 — ample Arrival InFp_ <br /> Samplc Transport; EXCOLCHEM Ctruri r I r,Ln�L�75xrICd ln; Ice Chesl <br /> Describe type of packing materials: None <br /> Has chilling pent ess begn[t? Yea Samples Received: On Ice <br /> Temp=ture of Samplcs(�C-)= f. Ice ChesL Tertlperature{2} ( C):_L <br /> Suction 2—Bottl&A nalysls Info. - -- <br /> Yas No KIA Carnnsentx <br /> Did all bottles arrive unbroken and i31L$CL? x <br /> Did all bolide lahelx agree wiLh COC? x _ <br /> W-12! r;vnlaiucrs tl*vd for the tests uesked? x <br /> were c43rrect escrvations used for the tests rcquosL.cd4 x <br /> Was a sufficient amount ofsatnplc sent Par renis indica[ed? x <br /> Were bubbles prexent in VOA Vials?:(Vol:ndle Mel hods Only) ( - <br /> Section 3 —Surnma/Flo regulator Info- <br /> glord S+aarmrs#: <br /> unuxed SUMM"11= <br /> Ite9ulat0r#: <br /> Wm;there any visual damage to surnma oanlsrets oe fl[sw eegu);norx4]:xpiiiin, <br /> Section 4—�Q� Irfa_ - <br /> Co[n Ieted Info Fmm Clem IciecL <br /> Yrs Nn Ca,nln;r.or - ... Yes Nu Camme[[ts <br /> Was COC Rt§celved }{ - r\n;li sin R uestad x - <br /> Daie Sampled }( - Sumroas urrlvcd wL[hin hpl{Lln&On5o X - <br /> irt[e :Lm Ig41 x - Any hold times less than 72 h" x - <br /> Sample ID x - Clieln Nftrrie X - <br /> Rash TAT x - Addres I-elephpnG V x - <br /> ;isctian 5—Comments f Discrepancies <br /> ;Nan C'liantnotillcd of discrepancies: N/A NQtitwd by; NIA <br /> Ex tanmions I Consmenm- <br /> k <br /> Samplcs I,al)[]e[L by: ZP Filled Date: 2{9117 <br /> Bin as; DPT_ i i cul <br /> by, Timo:09:14 <br /> C4)C S mnvWAnaMod by: Z+F. <br /> sample IabcLsrewiewed 3 <br /> oy: <br /> Excelchern Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> y custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />