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Table 4-1 Sample Analysis Plan <br /> Sample Analytes Container Preserved with Method <br /> Water <br /> Alkalinity 250 mL Poly 4°C EPA method 310.1 <br /> Inorganic Anions (Br, Cl, F, NO3/NO2, SO4) 250 mL Poly 4°C EPA method 300.1 <br /> Total Dissolved Solids 250 mL Poly 4°C EPA method 160.1 <br /> Total Metals 500 mL Poly HNO3 EPA method 6010/6020 <br /> Dissolved Metals' 500 mL Poly 4°C EPA method 6010/6020 <br /> Total Phosphate 250 mL Poly H2SO4 EPA method 365.2 <br /> Soil <br /> Chloride and Sulfate 1"x12"acetate sleeve 4°C EPA method 300.1 <br /> pH 1"x12" acetate sleeve 4°C EPA method 150.1 <br /> Total Metals2 1"x12" acetate sleeve 4°C EPA method 6010/6020 <br /> 1 - Lab filter and preserve <br /> 2-Total metals (soil) include Title 22 CAM17 metals (Ag, As, Ba, Be, Cd, Co, Cr, Cu, Hg, Mo, Ni, Pb, Sb, Se, <br /> Ti, V, Zn) plus Al, Ca, Mn, and Na <br />