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5.0 SAMPLE ANALYSES <br /> 5.1 General <br /> Analytical methods utilized by the certified analytical laboratory will follow EPA SW-846 <br /> requirements for the sampling of solid waste. Each of the samples will be analyzed for the <br /> following: <br /> Parameter Test Method <br /> ICP Metals (All) SW 6010B <br /> Total Halogens SW 9075 <br /> PCBs SW 8082 <br /> Corrosivity SW 1110A <br /> Flash Point SW 1010A <br /> Reactive Cyanide SW 9010B <br /> Reactive Sulfide SW 9030B <br /> Aquatic Toxicity CA Fish Bioassay <br /> 5.2 Quality Assurance/Quality Control <br /> Matrix Spike/Matrix Spike Duplicates — Laboratory Internal QA/QC <br /> Matrix spike and laboratory control samples will be obtained and analyzed to determine if <br /> sample recoveries falling outside of acceptance windows are attributed to sample matrix <br /> interferences and/or to laboratory errors, and to measure the accuracy of the analysis. <br /> Laboratory duplicates for inorganic analytes and matrix spike duplicates for organic analytes will <br /> be analyzed to evaluate laboratory reproducibility or precision. <br /> 6.0 REFERENCES <br /> CaIEPA, 2008. Sampling and Analysis Study of Treated Wood (Draft). Department of Toxic <br /> Substances Control, Toxics in Products Branch, Environmental Chemistry Laboratory. July. <br /> EPRI, 1995. Electric Power Research Institute. Management Practices for Used Treated <br /> Wood. TRI-104966, Research Project 2879-02. June. <br /> Mueller, J.G., P.J. Chapman, and R.H. Pritchard. 1989. Creosote-contaminated Sites. <br /> Environ. Science and Technology. Vol. 23. P. 1197-1201. <br /> Webb, D., 1989. Preservatives and Treatments for Utility Poles-Both Now and in the Future. In: <br /> Proceedings of International Conference on Wood Poles and Piles. For Collins, Colorado. <br /> October 25-27. p. E-13 to E-32. <br /> Used Oil Sampling and Analysis Plan 7 July 29, 2014 <br /> BNSF Railway Multiple Locations <br /> TRC Project No. 211983 <br />