|
EPA Method 1613
<br />PCDD/F ANALYTICAL LABORATORY
<br />FAL ID: 11455-001-OPR
<br />Date Extracted: 04-27-2018
<br />Client ID: OPR
<br />Date Received: NA
<br />Matrix: Solid
<br />Amount: 5.00 g
<br />Batch No: X4492
<br />51.6
<br />34.0-80.0
<br />Compound
<br />Conc
<br />QC Limits Qual
<br />2,3,7,8-TCDD
<br />10.8
<br />6.70-15.8
<br />1,2,3,7,8-PeCDD
<br />53.0
<br />35.0-71.0
<br />1,2,3,4,7,8-HxCDD
<br />47.7
<br />35.0-82.0
<br />1,2,3,6,7,8-HxCDD
<br />50.6
<br />38.0-67.0
<br />1,2,3,7,8,9-HxCDD
<br />47.5
<br />32.0-81.0
<br />1,2,3,4,6,7,8-HpCDD
<br />51.0
<br />35.0-70.0
<br />OCDD
<br />101
<br />78.0-144
<br />2,3,7,8-TCDF
<br />10.7
<br />7.50-15.8
<br />1,2,3,7,8-PeCDF
<br />50.3
<br />40.0-67.0
<br />2,3,4,7,8-PeCDF
<br />51.6
<br />34.0-80.0
<br />1,2,3,4,7,8-HxCDF
<br />51.1
<br />36.0-67.0
<br />1,2,3,6,7,8-HxCDF
<br />50.1
<br />42.0-65.0
<br />2,3,4,6,7,8-HxCDF
<br />51.1
<br />35.0-78.0
<br />1,2,3,7,8,9-HxCDF
<br />51.1
<br />39.0-65.0
<br />1,2,3,4,6,7,8-HpCDF
<br />51.1
<br />41.0-61.0
<br />1,2,3,4,7,8,9-HpCDF
<br />52.3
<br />39.0-69.0
<br />OCDF
<br />104
<br />63.0-170
<br />Internal Standards % Rec QC Limits
<br />13C -2,3,7,8-TCDD
<br />92.4
<br />20.0-175
<br />13C-1,2,3,7,8-PeCDD
<br />96.5
<br />21.0-227
<br />13C-1,2,3,4,7,8-HxCDD
<br />97.1
<br />21.0-193
<br />13C-1,2,3,6,7,8-HxCDD
<br />100
<br />25.0-163
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />88.8
<br />26.0-166
<br />13C-OCDD
<br />81.3
<br />13.0-198
<br />13C-2,3,7,8-TCDF
<br />97.6
<br />22.0-152
<br />13C-1,2,3,7,8-PeCDF
<br />91.3
<br />21.0-192
<br />13C-2,3,4,7,8-PeCDF
<br />92.6
<br />13.0-328
<br />13C-1,2,3,4,7,8-HxCDF
<br />89.0
<br />19.0-202
<br />13C-1,2,3,6,7,8-HxCDF
<br />90.0
<br />21.0-159
<br />13C-2,3,4,6,7,8-HxCDF
<br />88.6
<br />22.0-176
<br />13C-1,2,3,7,8,9-HxCDF
<br />87.6
<br />17.0-205
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />90.3
<br />21.0-158
<br />13C-1,2,3,4,7,8,9-HpCDF
<br />91.3
<br />20.0-186
<br />13C-OCDF
<br />80.4
<br />13.0-198
<br />Cleanup Surrogate
<br />37CI-2,3,7,8-TCDD 89.4 31.0 - 191
<br />Analyst:
<br />,
<br />Date: 5/1/2018
<br />Qual
<br />ICal: PCDDFAL4-12-20-17 Acquired: 04-30-2018
<br />GC Column: DB5MS 2005 WHO TEQ: NA
<br />Units: ng/ml
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />' Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000004 of 000022
<br />5172 Hillsdale Circle * EI Dorado Hills, CA 95762 ' Tel (916) 934-0900 " Fax (916) 934-0999 ' www.frontieranalytical.com
<br />
|