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EPA Method 1613 [�
<br />PCDD/F ANALYTICAL LABORATORY
<br />FAL ID: 11455 -001 -SA
<br />Date Extracted: 04-27-2018
<br />ICal: PCDDFAL4-12-20-17 Acquired: 04-30-2018
<br />Client ID: SP3-1
<br />Date Received: 04-12-2018
<br />GC Column:
<br />DBSMS
<br />2005 WHO TEQ: 1.79
<br />Matrix: Solid
<br />Amount: 5.01 g
<br />76.8
<br />Units: pg/g
<br />92.3
<br />Basis: Dry Weight
<br />Batch No: X4492
<br />% Solids: 92.26
<br />88.2
<br />21.0-178
<br />87.8
<br />26.0-152
<br />86.7
<br />26.0-123
<br />84.5
<br />2005
<br />82.5
<br />29.0-147
<br />Compound
<br />Conc DL
<br />Qual
<br />WHO Tox
<br />MDL
<br />Compound Conc DL Qua]
<br />2,3,7,8-TCDD
<br />ND 0.206
<br />-
<br />0.0273
<br />1,2,3,7,8-PeCDD
<br />0.545 -
<br />J
<br />0.545
<br />0.0570
<br />1,2,3,4,7,8-HxCDD
<br />0.893
<br />J
<br />0.0893
<br />0.0793
<br />1,2,3,6,7,8-HxCDD
<br />1.80 -
<br />J
<br />0.180
<br />0.0940
<br />Total TCDD ND 0.206
<br />1,2,3,7,8,9-HxCDD
<br />1.33
<br />J
<br />0.133
<br />0.0823
<br />Total PeCDD 4.20 - J
<br />1,2,3,4,6,7,8-HpCDD
<br />27.0
<br />0.270
<br />0.0842
<br />Total HxCDD 17.8
<br />OCDD
<br />194
<br />0.0582
<br />0.172
<br />Total HpCDD 55.7
<br />2,3,7,8-TCDF
<br />0.767
<br />J
<br />0.0767
<br />0.0269
<br />1,2,3,7,8-PeCDF
<br />ND 0.224
<br />-
<br />0.0449
<br />2,3,4,7,8-PeCDF
<br />0.672 -
<br />J
<br />0.202
<br />0.0468
<br />1,2,3,4,7,8-HxCDF
<br />0.658
<br />J
<br />0.0658
<br />0.0437
<br />1,2,3,6,7,8-HxCDF
<br />0.555
<br />J
<br />0.0555
<br />0.0417
<br />2,3,4,6,7,8-HxCDF
<br />0.473
<br />J
<br />0.0473
<br />0.0574
<br />1,2,3,7,8,9-HxCDF
<br />ND 0.202
<br />-
<br />0.0657
<br />Total TCDF 5.58
<br />1,2,3,4,6,7,8-HpCDF
<br />5.84 -
<br />0.0584
<br />0.0747
<br />Total PeCDF 3.97 J
<br />1,2,3,4,7,8,9-HpCDF
<br />0.735
<br />J
<br />0.00735
<br />0.0883
<br />Total HxCDF 8.08
<br />OCDF
<br />15.8
<br />0.00474
<br />0.170
<br />Tota] HpCDF 16.7
<br />Internal Standards
<br />13C -2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1,2, 3,4,7,8-HxCDD
<br />13C-1, 2, 3, 6, 7, 8-H xC D D
<br />13C-1, 2, 3, 4, 6, 7, 8-H pC D D
<br />13C-OCDD
<br />13C-2,3,7,8-TCDF
<br />13C-1,2, 3, 7,8-PeCDF
<br />13C-2,3,4,7,8-PeCDF
<br />13C-1,2,3,4,7,8-HxCDF
<br />13C-1,2,3,6,7,8-HxCDF
<br />13C-2, 3, 4, 6, 7, 8-HxC D F
<br />13C-1, 2, 3, 7, 8, 9-HxC D F
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />13C-1,2,3,4,7, 8,9-HpCDF
<br />13C-OCDF
<br />% Rec QC Limits Qual
<br />90.0
<br />25.0-164
<br />90.6
<br />25.0-181
<br />95.1
<br />32.0-141
<br />93.1
<br />28.0-130
<br />87.0
<br />23.0-140
<br />76.8
<br />17.0-157
<br />92.3
<br />24.0-169
<br />88.2
<br />24.0-185
<br />88.2
<br />21.0-178
<br />87.8
<br />26.0-152
<br />86.7
<br />26.0-123
<br />84.5
<br />28.0-136
<br />82.5
<br />29.0-147
<br />84.1
<br />28.0-143
<br />84.9
<br />26.0-138
<br />76.1
<br />17.0-157
<br />Cleanup Surrogate
<br />37C] -2,3,7,8-TCDD 88.4 35.0-197
<br />Analyst:
<br />Date: 5/1/2018
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />. Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000005 of 000022
<br />5172 Hillsdale Circle x EI Dorado Hills, CA 95762 ' Tel (916) 934-0900 ' Fax (916) 934-0999 " www.frontieranalytical.com
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