|
&M, EPA Method 1613
<br />PCDD/F ANALYTICAL LABORATORY
<br />FAL ID: 11455 -008 -SA
<br />Date Extracted: 04-27-2018
<br />ICal: PCDDFAL4-12-20-17 Acquired: 04-30-2018
<br />Client ID: SP3-8
<br />Date Received: 04-12-2018
<br />GC Column:
<br />DB51VIS
<br />2005 WHO TEQ: 1.34
<br />Matrix: Solid
<br />Amount: 5.01 g
<br />74.9
<br />Units: pg/g
<br />90.6
<br />Basis: Dry Weight
<br />Batch No: X4492
<br />% Solids: 93.69
<br />84.4
<br />21.0-178
<br />83.3
<br />26.0-152
<br />81.9
<br />26.0-123
<br />82.3
<br />2005
<br />82.3
<br />29.0-147
<br />Compound
<br />Cone DL
<br />Qual
<br />WHO Tox
<br />MDL
<br />Compound Cone DL Qual
<br />2,3,7,8-TCDD
<br />ND 0.243
<br />0.0273
<br />1,2,3,7,8-PeCDD
<br />ND 0.352
<br />0.0570
<br />1,2,3,4,7,8-HxCDD
<br />0.422 -
<br />J
<br />0.0422
<br />0.0793
<br />1,2,3,6,7,8-HxCDD
<br />1.29
<br />J
<br />0.129
<br />0.0940
<br />Total TCDD ND 0.243
<br />1,2,3,7,8,9-HxCDD
<br />1.00
<br />J
<br />0.100
<br />0.0823
<br />Total PeCDD ND 0.352
<br />1,2,3,4,6,7,8-HpCDD
<br />32.3
<br />0.323
<br />0.0842
<br />Total HxCDD 9.74 -
<br />OCDD
<br />267
<br />0.0801
<br />0.172
<br />Total HpCDD 56.5
<br />2,3,7,8-TCDF
<br />1.04 -
<br />0.104
<br />0.0269
<br />1,2,3,7,8-PeCDF
<br />ND 0.232
<br />-
<br />0.0449
<br />2,3,4,7,8-PeCDF
<br />0.654 -
<br />J
<br />0.196
<br />0.0468
<br />1,2,3,4,7,8-HxCDF
<br />1.10
<br />J
<br />0.110
<br />0.0437
<br />1,2,3,6,7,8-HxCDF
<br />0.615
<br />J
<br />0.0615
<br />0.0417
<br />2,3,4,6,7,8-HxCDF
<br />0.724
<br />J
<br />0.0724
<br />0.0574
<br />1,2,3,7,8,9-HxCDF
<br />ND 0.154
<br />-
<br />0.0657
<br />Total TCDF 5.68 M
<br />1,2,3,4,6,7,8-HpCDF
<br />10.2 -
<br />0.102
<br />0.0747
<br />Total PeCDF 6.52
<br />1,2,3,4,7,8,9-HpCDF
<br />0.794
<br />J
<br />0.00794
<br />0.0883
<br />Total HxCDF 11.3
<br />OCDF
<br />32.1
<br />0.00963
<br />0.170
<br />Total HpCDF 29.1
<br />Internal Standards
<br />13C -2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1,2,3,4,7,8-HxCDD
<br />13C-1,2, 3,6,7,8-HxCDD
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />13C-OCDD
<br />13C-2,3,7,8-TCDF
<br />13C-1,2, 3, 7,8-PeCDF
<br />13C-2,3,4,7,8-PeCDF
<br />13C-1,2,3,4,7, 8-HxCDF
<br />13C-1, 2, 3, 6, 7, 8-HxC D F
<br />13C-2, 3, 4, 6, 7, 8-HxC D F
<br />13C-1,2, 3, 7, 8, 9-HxCDF
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />13C-1,2,3,4, 7,8,9-HpCDF
<br />13C-OCDF
<br />Cleanup Surrogate
<br />37CI-2,3,7,8-TCDD
<br />Analyst: 9
<br />Date: 5/1/2018
<br />Rec QC Limits Qual
<br />87.6
<br />25.0-164
<br />88.4
<br />25.0-181
<br />92.9
<br />32.0-141
<br />88.5
<br />28.0-130
<br />84.8
<br />23.0-140
<br />74.9
<br />17.0-157
<br />90.6
<br />24.0-169
<br />83.7
<br />24.0-185
<br />84.4
<br />21.0-178
<br />83.3
<br />26.0-152
<br />81.9
<br />26.0-123
<br />82.3
<br />28.0-136
<br />82.3
<br />29.0-147
<br />82.4
<br />28.0-143
<br />84.6
<br />26.0-138
<br />78.1
<br />17.0-157
<br />84.5 35.0-197
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000012 of 000022
<br />5172 Hillsdale Circle " EI Dorado Hills, CA 95762 ` Tel (916) 934-0900 ` Fax (916) 934-0999 " www.frontieranalytical.com
<br />
|