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<br />EPA Method 1613 F&M.,
<br />PCDD/F ANALYTICAL LABORATORY
<br />FAL ID: 11455 -009 -SA
<br />Date Extracted: 04-27-2018
<br />ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />13C-1,2,3,7,8-PeCDD
<br />Client ID: SP3-9
<br />Date Received: 04-12-2018
<br />GC Column:
<br />DB5MS
<br />2005 WHO TEQ: 0.731
<br />13C-1,2,3,6,7,8-HxCDD
<br />Matrix: Solid
<br />Amount: 5.03 g
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />Units: pg/g
<br />23.0-140
<br />Basis: Dry Weight
<br />81.5
<br />Batch No: X4492
<br />% Solids: 92.21
<br />95.6
<br />24.0-169
<br />13C-1,2,3,7,8-PeCDF
<br />91.5
<br />24.0-185
<br />13C-2,3,4,7,8-PeCDF
<br />91.8
<br />21.0-178
<br />2005
<br />88.0
<br />26.0-152
<br />13C-1,2,3,6,7,8-HxCDF
<br />Compound
<br />Conc DL
<br />Qual
<br />WHO Tox
<br />MDL
<br />Compound Conc DL
<br />Qual
<br />2,3,7,8-TCDD
<br />0.470 -
<br />J
<br />0.470
<br />0.0273
<br />90.2
<br />26.0-138
<br />1,2,3,7,8-PeCDD
<br />ND 0.223
<br />17.0-157
<br />-
<br />0.0570
<br />1,2,3,4,7,8-HxCDD
<br />ND 0.170
<br />-
<br />0.0793
<br />1,2,3,6,7,8-HxCDD
<br />0.526 -
<br />J
<br />0.0526
<br />0.0940
<br />Total TCDD 0.470
<br />J
<br />1,2,3,7,8,9-HxCDD
<br />0.354
<br />J
<br />0.0354
<br />0.0823
<br />Total PeCDD 1.69
<br />J
<br />1,2,3,4,6,7,8-HpCDD
<br />8.05
<br />0.0805
<br />0.0842
<br />Total HxCDD 3.49
<br />J
<br />OCDD
<br />57.1
<br />0.0171
<br />0.172
<br />Total HpCDD 14.6
<br />2,3,7,8-TCDF
<br />0.546 -
<br />J
<br />0.0546
<br />0.0269
<br />1,2,3,7,8-PeCDF
<br />ND 0.179
<br />-
<br />0.0449
<br />2,3,4,7,8-PeCDF
<br />ND 0.180
<br />0.0468
<br />1,2,3,4,7,8-HxCDF
<br />ND 0.203
<br />0.0437
<br />1,2,3,6,7,8-HxCDF
<br />ND 0.212
<br />0.0417
<br />2,3,4,6,7,8-HxCDF
<br />ND 0.220
<br />0.0574
<br />1,2,3,7,8,9-HxCDF
<br />ND 0.235
<br />0.0657
<br />Total TCDF 1.29
<br />1,2,3,4,6,7,8-HpCDF
<br />1.82 -
<br />J
<br />0.0182
<br />0.0747
<br />Total PeCDF 1.00
<br />J
<br />1,2,3,4,7,8,9-HpCDF
<br />ND 0.173
<br />-
<br />0.0883
<br />Total HxCDF 1.77
<br />J
<br />OCDF
<br />7.04 -
<br />J
<br />0.00211
<br />0.170
<br />Total HpCDF 5.65
<br />Internal Standards % Rec QC Limits Qual
<br />13C -2,3,7,8-TCDD
<br />91.9
<br />25.0-164
<br />13C-1,2,3,7,8-PeCDD
<br />94.3
<br />25.0-181
<br />13C-1,2,3,4,7,8-HxCDD
<br />97.8
<br />32.0-141
<br />13C-1,2,3,6,7,8-HxCDD
<br />95.7
<br />28.0-130
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />91.1
<br />23.0-140
<br />13C-OCDD
<br />81.5
<br />17.0-157
<br />13C-2,3,7,8-TCDF
<br />95.6
<br />24.0-169
<br />13C-1,2,3,7,8-PeCDF
<br />91.5
<br />24.0-185
<br />13C-2,3,4,7,8-PeCDF
<br />91.8
<br />21.0-178
<br />13C-1,2,3,4,7,8-HxCDF
<br />88.0
<br />26.0-152
<br />13C-1,2,3,6,7,8-HxCDF
<br />85.7
<br />26.0-123
<br />13C-2,3,4,6,7,8-HxCDF
<br />87.3
<br />28.0-136
<br />13C-1,2,3,7,8,9-HxCDF
<br />86.4
<br />29.0-147
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />88.1
<br />28.0-143
<br />13C-1,2,3,4,7,8,9-HpCDF
<br />90.2
<br />26.0-138
<br />13C-OCDF
<br />82.4
<br />17.0-157
<br />Cleanup Surrogate
<br />37CI-2,3,7,8-TCDD 85.7 35.0-197
<br />Analyst: 9
<br />Date: 5/1/2018
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />' Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000013 of 000022
<br />5172 Hillsdale Circle' El Dorado Hills, CA 95762' Tel (916) 934-0900' Fax (916) 934-0999 `www,frontieranalytical.com
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