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EPA Method 1613 &M,
<br />PCDD/F ANALYTICAL LABORATORY
<br />FAL ID: 11455 -011 -SA
<br />Date Extracted: 04-27-2018
<br />ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: SP3-11
<br />Date Received: 04-12-2018
<br />GC Column:
<br />DB51VIS
<br />2005 WHO TEQ: 0.616
<br />Matrix: Solid
<br />Amount: 5.02 g
<br />Units: pg/g
<br />Basis: Dry Weight
<br />Batch No: X4492
<br />% Solids: 92.68
<br />2005
<br />Compound
<br />Cone DL
<br />Qual
<br />WHO Tox
<br />MDL
<br />Compound Cone DL Qual
<br />2,3,7,8-TCDD
<br />ND 0.221
<br />0.0273
<br />1,2,3,7,8-PeCDD
<br />ND 0.283
<br />0.0570
<br />1,2,3,4,7,8-HxCDD
<br />ND 0.254
<br />0.0793
<br />1,2,3,6,7,8-HxCDD
<br />0.963 -
<br />J
<br />0.0963
<br />0.0940
<br />Total TCDD ND 0.221
<br />1,2,3,7,8,9-HxCDD
<br />0.676
<br />J
<br />0.0676
<br />0.0823
<br />Total PeCDD ND 0.283
<br />1,2,3,4,6,7,8-HpCDD
<br />16.7
<br />0.167
<br />0.0842
<br />Total HxCDD 5.96 -
<br />OCDD
<br />139
<br />0.0417
<br />0.172
<br />Total HpCDD 31.3
<br />2,3,7,8-TCDF
<br />0.516 -
<br />J
<br />0.0516
<br />0.0269
<br />1,2,3,7,8-PeCDF
<br />ND 0.247
<br />-
<br />0.0449
<br />2,3,4,7,8-PeCDF
<br />ND 0.264
<br />-
<br />0.0468
<br />1,2,3,4,7,8-HxCDF
<br />0.372 -
<br />J
<br />0.0372
<br />0.0437
<br />1,2,3,6,7,8-HxCDF
<br />0.374
<br />J
<br />0.0374
<br />0.0417
<br />2,3,4,6,7,8-HxCDF
<br />0.374
<br />J
<br />0.0374
<br />0.0574
<br />1,2,3,7,8,9-HxCDF
<br />0.337
<br />J
<br />0.0337
<br />0.0657
<br />Total TCDF 1.88
<br />1,2,3,4,6,7,8-HpCDF
<br />3.84
<br />J
<br />0.0384
<br />0.0747
<br />Total PeCDF 1.73 J
<br />1,2,3,4,7,8,9-HpCDF
<br />0.460
<br />J
<br />0.00460
<br />0.0883
<br />Total HxCDF 5.04
<br />OCDF
<br />11.7
<br />0.00351
<br />0.170
<br />Total HpCDF 11.1
<br />Internal Standards % Rec
<br />13C -2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1,2,3,4,7,8-HxCDD
<br />13C-1,2,3,6,7,8-HxCDD
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />13C-OCDD
<br />13C-2, 3, 7, 8-TCDF
<br />13C-1,2,3,7,8-PeCDF
<br />13C-2,3,4,7,8-PeCDF
<br />13C-1,2, 3,4,7,8-HxCDF
<br />13C-1,2,3,6,7,8-HxCDF
<br />13C-2,3,4,6,7, 8-HxCDF
<br />13C-1, 2, 3, 7, 8, 9-HxC D F
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />13C-1,2,3,4,7,8,9-HpCDF
<br />13C-OCDF
<br />Cleanup Surrogate
<br />37CI-2,3,7,8-TCDD
<br />Analyst: 9
<br />Date: 5/1/2018
<br />90.6
<br />96.3
<br />101
<br />96.8
<br />92.4
<br />85.1
<br />96.9
<br />88.6
<br />89.6
<br />90.9
<br />88.4
<br />89.2
<br />87.7
<br />88.4
<br />89.8
<br />83.0
<br />QC Limits Qual
<br />25.0-164
<br />25.0-181
<br />32.0-141
<br />28.0-130
<br />23.0-140
<br />17.0-157
<br />24.0-169
<br />24.0-185
<br />21.0-178
<br />26.0-152
<br />26.0-123
<br />28.0-136
<br />29.0-147
<br />28.0-143
<br />26.0-138
<br />17.0-157
<br />87.9 35.0-197
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000015 of 000022
<br />5172 Hillsdale Circle * EI Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
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