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FAL ID: 11455 -012 -SA
<br />Client ID: SP3-12
<br />Matrix: Solid
<br />Batch No: X4492
<br />Compound
<br />2,3,7,8-TCDD
<br />1,2,3,7,8-PeCDD
<br />1,2,3,4,7,8-HxCDD
<br />1,2,3,6,7,8-HxCDD
<br />1,2,3,7,8,9-HxCDD
<br />1,2,3,4,6,7,8-HpCDD
<br />OCDD
<br />2,3,7,8-TCDF
<br />1,2,3,7,8-PeCDF
<br />2,3,4,7,8-PeCDF
<br />1,2, 3,4,7, 8-HxCDF
<br />1,2,3,6,7,8-HxCDF
<br />2,3,4,6,7,8-HxCDF
<br />1,2,3,7,8,9-HxCDF
<br />1,2,3,4,6,7,8-HpCDF
<br />1,2,3,4,7,8,9-HpCDF
<br />OCDF
<br />Internal Standards
<br />13C -2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1,2, 3,4,7,8-HxCDD
<br />13C-1,2, 3,6,7,8-HxCDD
<br />13C-1,2,3,4,6,7,8-HpCDD
<br />13C-OCDD
<br />13C-2,3,7,8-TCDF
<br />13C-1,2,3,7,8-PeCDF
<br />13C-2,3,4,7,8-PeCDF
<br />13C-1,2,3,4, 7,8-HxCDF
<br />13C-1,2, 3,6,7, 8-HxCDF
<br />13C-2,3,4,6,7,8-HxCDF
<br />13C-1,2,3,7,8,9-HxCDF
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />13C-1,2,3,4,7,8,9-HpCDF
<br />13C-OCDF
<br />URM.,
<br />EPA Method 1613
<br />PCDD/F ANALYTICAL LABORATORY
<br />Date Extracted: 04-27-2018
<br />ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Date Received: 04-12-2018
<br />GC Column:
<br />DB5MS
<br />2005 WHO TEQ: 1.79
<br />Amount: 5.03 g
<br />Units: pg/g
<br />Basis: Dry Weight
<br />% Solids: 94.10
<br />2005
<br />Cone DL
<br />Qual
<br />WHO Tox
<br />MDL
<br />Compound Cone DL Qual
<br />ND 0.229
<br />0.0273
<br />ND 0.384
<br />0.0570
<br />ND 0.267
<br />0.0793
<br />2.30 -
<br />J
<br />0.230
<br />0.0940
<br />Total TCDD 0.432 - J
<br />1.11
<br />J
<br />0.111
<br />0.0823
<br />Total PeCDD ND 0.384
<br />46.8
<br />0.468
<br />0.0842
<br />Total HxCDD 16.3 -
<br />395
<br />0.119
<br />0.172
<br />Total HpCDD 82.1
<br />1.12
<br />0.112
<br />0.0269
<br />ND 0.271
<br />-
<br />0.0449
<br />0.896 -
<br />J
<br />0.269
<br />0.0468
<br />1.24
<br />J
<br />0.124
<br />0.0437
<br />1.22
<br />J
<br />0.122
<br />0.0417
<br />0.904
<br />J
<br />0.0904
<br />0.0574
<br />0.422
<br />J
<br />0.0422
<br />0.0657
<br />Total TCDF 6.85
<br />8.09
<br />0.0809
<br />0.0747
<br />Total PeCDF 4.91 J
<br />1.54
<br />J
<br />0.0154
<br />0.0883
<br />Total HxCDF 9.17
<br />14.6
<br />0.00438
<br />0.170
<br />Total HpCDF 17.9
<br />% Rec QC Limits Qual
<br />78.4 25.0-164
<br />86.6 25.0-181
<br />88.3 32.0-141
<br />84.9 28.0-130
<br />80.1 23.0-140
<br />73.7 17.0-157
<br />79.7 24.0-169
<br />81.9 24.0-185
<br />83.1 21.0-178
<br />78.6 26.0-152
<br />77.3 26.0-123
<br />77.8 28.0-136
<br />75.6 29.0-147
<br />77.0 28.0-143
<br />78.5 26.0-138
<br />71.7 17.0-157
<br />Cleanup Surrogate
<br />37CI-2,3,7,8-TCDD 74.4 35.0-197
<br />Analyst: 9
<br />Date: 5/1/2018
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000016 of 000022
<br />5172 Hillsdale Circle EI Dorado Hills, CA 95762 k Tel (916) 934-0900 ` Fax (916) 934-0999 ' www.frontieranalytical.com
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