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FAL ID: 11455 -013 -SA
<br />Client ID: SP4-1
<br />Matrix: Solid
<br />Batch No: X4492
<br />Compound
<br />2,3,7,8-TCDD
<br />1,2,3,7,8-PeCDD
<br />1,2,3,4,7,8-HxCDD
<br />1,2,3,6,7,8-HxCDD
<br />1,2,3,7,8,9-HxCDD
<br />1,2,3,4,6,7,8-HpCDD
<br />OCDD
<br />2,3,7,8-TCDF
<br />1,2, 3,7,8-PeCDF
<br />2,3,4,7,8-PeCDF
<br />1,2,3,4, 7,8-HxCDF
<br />1,2,3,6,7,8-HxCDF
<br />2,3,4,6,7,8-HxCDF
<br />1,2,3,7,8,9-HxCDF
<br />1,2,3,4,6,7,8-HpCDF
<br />1,2,3,4,7,8,9-HpCDF
<br />OCDF
<br />Internal Standards
<br />13C -2,3,7,8-TCDD
<br />13C-1,2,3,7,8-PeCDD
<br />13C-1, 2, 3,4, 7, 8-HxCDD
<br />13C-1, 2, 3, 6, 7, 8-H xC D D
<br />13C-1,2,3,4,6,7, 8-HpCDD
<br />13C-OCDD
<br />13C-2,3,7,8-TCDF
<br />13C-1,2, 3, 7,8-PeCDF
<br />13C-2,3,4,7,8-PeCDF
<br />13C-1,2,3,4,7,8-HxCDF
<br />13C-1,2,3,6,7,8-HxCDF
<br />13C-2,3,4,6,7, 8-HxCDF
<br />13C-1,2,3, 7, 8,9-HxCDF
<br />13C-1,2,3,4,6,7,8-HpCDF
<br />13C-1,2,3,4,7,8,9-HpCDF
<br />13C-OCDF
<br />Cleanup Surrogate
<br />37C1 -2,3,7,8-TCDD
<br />Analyst: 9
<br />Date: 5/1/2018
<br />EPA Method 1613 [�
<br />PCDD/F ANALYTICAL LABORATORY
<br />Date Extracted: 04-27-2018
<br />Date Received: 04-12-2018
<br />Amount: 5.04 g
<br />% Solids: 96.08
<br />Cone
<br />ND
<br />ND
<br />0.471
<br />4.20
<br />1.88
<br />79.8
<br />683
<br />1.73
<br />0.461
<br />1.02
<br />1.81
<br />1.98
<br />1.53
<br />0.615
<br />13.8
<br />2.31
<br />24.5
<br />Rec
<br />88.8
<br />92.7
<br />92.9
<br />89.9
<br />86.4
<br />78.9
<br />94.0
<br />89.8
<br />92.5
<br />81.9
<br />81.2
<br />80.1
<br />82.0
<br />82.5
<br />86.5
<br />78.1
<br />DL Qual
<br />0.184
<br />0.309
<br />J
<br />J
<br />J
<br />QC Limits
<br />25.0-164
<br />25.0-181
<br />32.0-141
<br />28.0-130
<br />23.0-140
<br />17.0-157
<br />24.0-169
<br />24.0-185
<br />21.0-178
<br />26.0-152
<br />26.0-123
<br />28.0-136
<br />29.0-147
<br />28.0-143
<br />26.0-138
<br />17.0-157
<br />85.3 35.0-197
<br />J
<br />J
<br />J
<br />J
<br />J
<br />J
<br />J
<br />Qual
<br />]Cal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />GC Column:
<br />DBSMS
<br />2005 WHO TEQ: 2.91
<br />Units: pg/g
<br />Basis: Dry Weight
<br />2005
<br />WHO Tox
<br />MDL
<br />Compound Cone DL Qual
<br />0.0273
<br />0.0570
<br />0.0471
<br />0.0793
<br />0.420
<br />0.0940
<br />Total TCDD 0.754 J
<br />0.188
<br />0.0823
<br />Total PeCDD 1.40 J
<br />0.798
<br />0.0842
<br />Total HxCDD 32.4
<br />0.205
<br />0.172
<br />Total HpCDD 150
<br />0.173
<br />0.0269
<br />0.0138
<br />0.0449
<br />0.306
<br />0.0468
<br />0.181
<br />0.0437
<br />0.198
<br />0.0417
<br />0.153
<br />0.0574
<br />0.0615
<br />0.0657
<br />Total TCDF 12.4
<br />0.138
<br />0.0747
<br />Total PeCDF 7.70
<br />0.0231
<br />0.0883
<br />Total HxCDF 16.5
<br />0.00735
<br />0.170
<br />Total HpCDF 31.6
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre -filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />Reviewed By:
<br />Date: 5/1/2018
<br />000017 of 000022
<br />5172 Hillsdale Circle * EI Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
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