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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11472-002-SA Date Extracted: 04-30-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: SP5-2 Date Received: 04-13-2018 GC Column: DB5MS 2005 WHO TEQ: 0.670
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4493 % Solids: 92.60
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.189 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.287 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.213 -0.0793
<br />1,2,3,6,7,8-HxCDD 0.736 - J 0.0736 0.0940 Total TCDD ND 0.189
<br />1,2,3,7,8,9-HxCDD 0.589 - J 0.0589 0.0823 Total PeCDD ND 0.287
<br />1,2,3,4,6,7,8-HpCDD 10.9 -0.109 0.0842 Total HxCDD 5.21 -
<br />OCDD 73.3 - 0.0220 0.172 Total HpCDD 20.4 -
<br />2,3,7,8-TCDF 0.829 - J 0.0829 0.0269
<br />1,2,3,7,8-PeCDF 0.269 - J 0.00807 0.0449
<br />2,3,4,7,8-PeCDF 0.478 - J 0.143 0.0468
<br />1,2,3,4,7,8-HxCDF 0.572 - J 0.0572 0.0437
<br />1,2,3,6,7,8-HxCDF 0.459 - J 0.0459 0.0417
<br />2,3,4,6,7,8-HxCDF 0.407 - J 0.0407 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.159 -0.0657 Total TCDF 4.70 -
<br />1,2,3,4,6,7,8-HpCDF 2.66 - J 0.0266 0.0747 Total PeCDF 4.34 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.246 -0.0883 Total HxCDF 4.67 -J
<br />OCDF 5.95 - J 0.00179 0.170 Total HpCDF 6.39 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 85.9 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 93.1 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 112 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 108 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 98.8 23.0 - 140
<br />13C-OCDD 89.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 82.8 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 94.7 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 94.6 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 103 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 99.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 98.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 88.7 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 80.9 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 85.6 26.0 - 138
<br />13C-OCDF 84.9 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 76.2 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/2/2018 5/2/2018
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