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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11472-003-SA Date Extracted: 04-30-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: SP5-3 Date Received: 04-13-2018 GC Column: DB5MS 2005 WHO TEQ: 1.24
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4493 % Solids: 90.60
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.204 - 0.0273
<br />1,2,3,7,8-PeCDD 0.340 - J 0.340 0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.279 -0.0793
<br />1,2,3,6,7,8-HxCDD 0.910 - J 0.0910 0.0940 Total TCDD 0.472 -J
<br />1,2,3,7,8,9-HxCDD 0.499 - J 0.0499 0.0823 Total PeCDD 2.65 -J
<br />1,2,3,4,6,7,8-HpCDD 12.7 -0.127 0.0842 Total HxCDD 6.81 -
<br />OCDD 82.4 - 0.0247 0.172 Total HpCDD 24.6 -
<br />2,3,7,8-TCDF 1.04 -0.104 0.0269
<br />1,2,3,7,8-PeCDF 0.272 - J 0.00816 0.0449
<br />2,3,4,7,8-PeCDF 0.747 - J 0.224 0.0468
<br />1,2,3,4,7,8-HxCDF 0.920 - J 0.0920 0.0437
<br />1,2,3,6,7,8-HxCDF 0.565 - J 0.0565 0.0417
<br />2,3,4,6,7,8-HxCDF 0.484 - J 0.0484 0.0574
<br />1,2,3,7,8,9-HxCDF 0.372 - J 0.0372 0.0657 Total TCDF 5.58 -
<br />1,2,3,4,6,7,8-HpCDF 2.91 - J 0.0291 0.0747 Total PeCDF 5.24 -M
<br />1,2,3,4,7,8,9-HpCDF 0.556 - J 0.00556 0.0883 Total HxCDF 6.19 -
<br />OCDF 5.75 - J 0.00173 0.170 Total HpCDF 7.89 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 81.6 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 90.1 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 112 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 110 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 97.8 23.0 - 140
<br />13C-OCDD 91.7 17.0 - 157
<br />13C-2,3,7,8-TCDF 80.4 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 95.3 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 98.1 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 102 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 99.8 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 96.1 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 88.5 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 84.6 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 83.3 26.0 - 138
<br />13C-OCDF 88.4 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 73.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/2/2018 5/2/2018
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