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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: Scrubber Ball Profile <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 01/25/2108:41 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AAJ0292-EPA 7471A <br /> Matrix Spike(AAJ0292-MS1) Source:2010157-01 Prepared&Analyzed: 10/26/20 <br /> Mercury 0.218 0.016 mg/kg 0.200 0.00600 106 75-125 <br /> Matrix Spike Dup(AAJ0292-MSD1) Source:2010157-01 Prepared&Analyzed: 10/26/20 <br /> Mercury 0.214 0.016 mg/kg 0.200 0.00600 104 75-125 1.48 20 <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 7 of 10 <br />