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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: Scrubber Ball Profile <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 01/25/2108:41 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AAK0018-EPA 7470A <br /> Blank(A A K0018-BLK1) Prepared&Analyzed: 11/02/20 <br /> Mercury ND 0.0160 mg/L <br /> LCS(A A K0018-BS1) Prepared&Analyzed: 11/02/20 <br /> Mercury 0.170 0.0160 mg/L 0.200 85.2 75-120 <br /> LCS Dup(AAK0018-BSD1) Prepared&Analyzed: 11/02/20 <br /> Mercury 0.162 0.0160 1119/1- 0.200 80.8 75-120 5.30 20 <br /> Matrix Spike(AAK0018-MS1) Source:2010207-01 Prepared&Analyzed: 11/02/20 <br /> Mercury 0.162 0.0160 mg/L 0.200 ND 81.2 75-125 <br /> Matrix Spike Dup(AAK0018-MSD1) Source:2010207-01 Prepared&Analyzed: 11/02/20 <br /> Mercury 0.165 0.0160 mg/L 0.200 ND 82.4 75-125 1.47 20 <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 8 of 10 <br />