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QC Sample Results <br /> Client: Patriot Environmental Services Job ID: 440-250736-1 <br /> Project/Site: French Camp <br /> Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) <br /> Lab Sample ID: LCSD 440-570836/3-B Client Sample ID: Lab Control Sample Dup <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 570955 Prep Batch: 570836 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> Isophorone 2500 1890 ug/Kg 75 38-119 3 35 <br /> Naphthalene 2500 1830 ug/Kg 73 42-115 1 35 <br /> Nitrobenzene 2500 1770 ug/Kg 71 38-116 0 35 <br /> N-Nitrosodi-n-propylamine 2500 1730 ug/Kg 69 31-124 2 35 <br /> N-Nitrosodiphenylamine 2500 2010 ug/Kg 80 48-130 3 35 <br /> Pentachlorophenol 5000 4580 ug/Kg 92 40-121 2 35 ' <br /> Phenanthrene 2500 1900 ug/Kg 76 51-122 6 35 <br /> Phenol 2500 1780 ug/Kg 71 42-133 2 35 <br /> Pyrene 2500 2020 ug/Kg 81 54-127 7 35 <br /> bis(2-chloroisopropyl)ether 2500 1400 ug/Kg 56 25-116 1 35 <br /> N-Nitrosodimethylamine 2500 1610 ug/Kg 65 28-107 4 35 <br /> Pyridine 5000 2520 ug/Kg 50 21-76 6 35 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 2-Fluorobiphenyl 77 42-113 <br /> 2-Fluorophenol(Surr) 69 18-138 <br /> 2,4,6-Tribromophenol(Surr) 93 10-147 <br /> Nitrobenzene-d5(Surr) 71 39-104 <br /> Terphenyl-d14(Surr) 85 43-125 <br /> Phenol-d6(Surr) 70 37-125 <br /> Method: 8015B - Gasoline RangeOrganics - (GC) <br /> Lab Sample ID: MB 440-572082/5 Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 572082 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> GRO(C4-C12) ND 40000 20000 ug/Kg 10/02/19 11:40 100 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 4-Bromofluorobenzene(Surr) 118 65-140 10/02/19 1140 100 <br /> Lab Sample ID: LCS 440-572082/41 Client Sample ID: Lab Control Sample <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 572082 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> GRO(C4-C12) 160000 160000 ug/Kg 100 70-135 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Surr) 110 65-140 <br /> Eurofins TestAmerica, Irvine <br /> Page 21 of 31 10/7/2019 <br />