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QC Sample Results <br /> Client: Patriot Environmental Services Job ID: 440-250736-1 <br /> Project/Site: French Camp <br /> Method: 8015B - Gasoline Range Organics (GC) (Continued) <br /> Lab Sample ID: LCSD 440-572082/4 Client Sample ID: Lab Control Sample Dup <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 572082 <br /> Spike LCSD LCSD %Rec. RPD <br /> Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> GRO(C4-C12) 160000 176000 ug/Kg 110 70-135 9 20 <br /> LCSD LCSD <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene(Surr) 117 65-140 <br /> --— - -- ........... ....... _..------ — --- - —----- — ._.. -- - <br /> Method: 8015B - Diesel Range Organics (DRO) (GC) <br /> Lab Sample ID: MB 440-571667/1-A Client Sample ID: Method Blank <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 571645 Prep Batch: 571667 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> C13-C22 ND 5.0 2.5 mg/Kg 09/30/19 13:33 10/01/19 09:05 1 <br /> C23-C40 2.60 J 5.0 2.5 mg/Kg 09/30/19 13:33 10/01/19 09:05 1 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> n-Octacosane 87 40-140 09/30/19 1333 10/01/19 0905 1 <br /> Lab Sample ID: LCS 440-571667/2-A Client Sample ID: Lab Control Sample <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 571645 Prep Batch: 571667 <br /> Spike LCS LCS %Rec. <br /> Analyte Added Result Qualifier Unit D %Rec Limits <br /> C10-C28 66.7 60.5 mg/Kg 91 45-115 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> n-Octacosane 86 40-140 <br /> Lab Sample ID:440-250886-C-7-E MS Client Sample ID: Matrix Spike <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 571645 Prep Batch: 571667 <br /> Sample Sample Spike MS MS %Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits <br /> C10-C28 23 B 66.5 82.8 mg/Kg 91 40-120 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> n-Octacosane 85 40-140 <br /> Lab Sample ID: 440-250886-C-7-F MSD Client Sample ID: Matrix Spike Duplicate <br /> Matrix: Solid Prep Type: Total/NA <br /> Analysis Batch: 571645 Prep Batch: 571667 <br /> Sample Sample Spike MSD MSD %Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit <br /> C10-C28 23 B 66.5 81.4 mg/Kg 89 40-120 2 30 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> n-Octacosane 84 40-140 <br /> Eurofins TestAmerica, Irvine <br /> Page 22 of 31 10/7/2019 <br />