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Soil samples for volatile compounds such as TPHg and VOCs will be collected, in <br />accordance with the 5035-preparation method (EnCoreTM sampler). Upon sample retrieval, an <br />EnCoreTM sampling device will be pushed into the exposed leading end of the sample liner. As <br />the EnCoreTM device is pushed, an internal piston retracts allowing soil to fill a cylinder to a <br />capacity of either 5 gram (g) or 25g of soil mass, thus preventing formation of head space above <br />the soil within the sampling device. If, during sampling it is not possible to immediately collect <br />soil using the EnCoreTM sampling device, the end of the acetate liner will be capped with a Teflon <br />sheet and a plastic end cap to prevent the loss of volatiles. Once collected, the EnCoreTM sample <br />device will be capped with a locking cap fitted with an "0-ring" seal to prevent loss of volatiles, <br />and will then be placed into a previously labeled foil pouch and sealed. Prior to placing the <br />EnCoreTM sampling device into the foil pouch, a self-adhesive labeled seal is placed onto the <br />locking mechanism to secure it from tampering, and to act as additional field QC of the sample. <br />The secured sample is then placed into a re-sealable plastic bag and put into the insulated chest <br />filled with water ice pending transport to a California certified laboratory for analysis. <br />Soil samples for low- or non-volatile compounds as TPHd, TPHo, SVOCs, metals, PCBs and <br />pH will be collected using the soil within the sample liner. If the sample liner is acetate, <br />approximately six (6) inches of sample liner will be cut from the leading end, and the exposed <br />ends of the liner will be capped with Teflon sheeting and secured with plastic end caps. If either <br />brass or stainless steel, the leading 6-inch long liner will be similarly capped and secured. The <br />sample will then be labeled, placed into a re-sealable plastic bag, and placed into the insulated <br />chest filled with water ice pending transport to a California certified laboratory for analysis. If <br />insufficient soil sample is collected, either an additional sample will be collected from the <br />borehole beginning where the last sample was collected, or the rig will be moved 18 to 24 inches <br />from the initial borehole and sampling will continue at the target depth. <br />Remaining soil will be placed into a re-sealable plastic bag and set aside for approximately <br />two (2) to five (5) minutes, after which time a measure of VOCs will be made using a portable <br />photoionization detector (HD) or equivalent organic vapor analyzer. The soil will then be <br />described by a California Professional Geologist in accordance with the Unified Soil <br />Classification System (USCS) method of soil description. <br />A mobile laboratory may be used during sampling to analyze the samples onsite. If used, <br />additional analysis may be performed by the mobile laboratory at depths other than initially <br />selected to assist in vertical delineation. In addition, sampling may be advanced at other locations <br />to further delineate petroleum hydrocarbons and/or VOCs. The necessity for additional sampling <br />at other locations may also be indicated by high VOC measurements on the PID. The selection of <br />additional sample locations will be at the discretion of the Professional Geologist responsible for <br />this project. <br />The indicated analysis for the PCOCs and COCs at the identified depths is a guideline and <br />may be analyzed at other than their pre-selected depths to further characterize the PCOCs <br />depending on the results of the initial laboratory analysis. Selection of additional analysis will be <br />at the discretion of the Professional Geologist responsible for this project. <br />Golden State Environmental, Inc. - 19 - Los Angeles, San Diego and Houston <br />Revised Work Plan — Soil and GW Characterization July 2006