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Al <br />rc7,- <br />ETc <br />r-S7 <br />1 <br />7C-171 <br />FST-- <br />WG1465900 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. at <br />Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1210848-01,02,03,04,05 <br />Laboratory Control Sample (LCS) <br />(LCS) R3522031-1 04/2 5/20 04:10 <br />Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier <br />Analyte mg/kg mg/kg % % <br />2,4-Dimethylphenol 0.666 0.367 55.1 15.0-120 <br />4,6-Dinitro-2-methylphenol 0.666 0.388 58.3 16.0-120 <br />2,4-Dinitrophenol 0.666 0.253 38.0 10.0-120 <br />2-Nitrophenol 0.666 0.360 54.1 20.0-120 <br />4-Nitrophenol 0.666 0.436 65.5 27.0-120 <br />Pentachlorophenol 0.666 0.464 69.7 29.0-120 <br />Phenol 0.666 0.416 62.5 28.0-120 <br />2,4,5-Trichlorophenol 0.666 0.473 71.0 38.0-120 <br />2,4,6-Trichlorophenol 0.666 0.471 70.7 37.0-120 <br />(S) Nitrobenzene-d5 48.6 10.0-122 <br />(S) 2-Fluorobiphenyl 61.3 15.0-120 <br />(S) p-Terphenyl-d14 64.3 10.0-120 <br />(S) Phenol-d5 62.2 10.0-120 <br />(S) 2-Fluorophenol 66.7 12.0-120 <br />(S) Z4,6-Tribromophenol 76.3 10.0-127 <br />L1210848-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) 9 SC <br />(OS) L1210848-02 04/25/20 06:35 • (MS) R3522031-3 04/25/20 06:55 • (MSD) R3522031-4 04/25/20 07:16 <br />Spike Amount Original Result MSD Result MS Result (dry) MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits (dry) (dry) (dry) <br />Analyte mg/kg mg/kg mg/kg mg/kg <br />Acenaphthene 0.745 U 0.399 0.403 <br />Acenaphthylene 0.745 u 0.463 0.453 <br />Anthracene 0.745 U 0.447 0.434 <br />Benzidine 1.49 U 0.159 0.142 <br />Benzo(a)anthracene 0.745 U 0.491 0.508 <br />Benzo(b)fluoranthene 0.745 u 0.467 0.458 <br />Benzo(k)fluoranthene 0.745 u 0.421 0.426 <br />Benzo(g,h,i)perylene 0.745 0.00778 0.536 0.493 <br />Benzo(a)pyrene 0.745 U 0.486 0.477 <br />Bis(2-chlorethoxy)methane 0.745 u 0.355 0.360 <br />Bis(2-chloroethyl)ether 0.745 U 0.380 0.395 <br />2,2-Oxybis(1-Chloropropane) 0.745 u 0.352 0.323 <br />4-Bromophenyl-phenylether 0.745 U 0.501 0.522 <br />2-Chloronaphthalene 0.745 U 0.422 0.410 <br />4-Chlorophenyl-phenylether 0.745 U 0.439 0.428 <br />Chrysene 0.745 U 0.449 0.437 <br />Dibenz(a,h)anthracene 0.745 U 0.508 0.516 <br />1,2-Dichlorobenzene 0.745 U 0.349 0.328 <br />% % % % % <br />53.5 54.0 1 18.0-120 1.13 32 <br />62.2 60.6 1 25.0-120 2.23 32 <br />60.1 58.1 1 22.0-120 3.09 29 <br />10.7 9.47 1 10.0-120 J6 11.3 40 <br />65.9 67.9 1 25.0-120 3.41 29 <br />62.7 61.2 1 19.0-122 1.97 31 <br />56.6 57.0 1 23.0-120 1.07 30 <br />70.9 64.9 1 10.0-120 8.39 33 <br />65.2 63.8 1 24.0-120 1.89 30 <br />47.7 48.2 1 10.0-120 1.27 34 <br />51.1 52.9 1 10.0-120 3.81 40 <br />47.3 43.2 1 10.0-120 8.75 40 <br />67.2 69.9 1 27.0-120 4.22 30 <br />56.7 54.9 1 20.0-120 3.00 32 <br />59.0 57.3 1 24.0-120 2.62 29 <br />60.2 58.5 1 21.0-120 2.56 29 <br />68.1 69.0 1 10.0-120 1.55 32 <br />46.8 43.9 1 10.0-120 6.04 38 <br />ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: