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Ss Mk Sr Cp 2 Tc WG1465900 QUALITY Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1210848-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike CONTROL SUMMARY L1210848-01,02,03,04,05 ONE LAB NATIONWIDE Duplicate (MSD) (OS) L1210848-02 04/25/20 06:35 • (MS) R3522031-3 04/25/20 06:55 • (MSD) R3522031-4 04/25/20 07:16 Spike Amount (dry) Original Result (dry) MSD Result MS Result (dry) MS Rec. MSD Rec. (dry) Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg % % % % % 1,3-Dichlorobenzene 0.745 U 0.342 0.326 45.9 43.6 1 10.0-120 4.76 40 14-Dichlorobenzene 0.745 U 0.333 0.328 44.7 43.9 1 10.0-120 1.37 39 3,3-Dichlorobenzidine 1.49 U 1.03 0.991 69.5 66.1 1 10.0-120 4.15 34 2,4-Dinitrotoluene 0.745 U 0.470 0.517 63.1 69.1 1 30.0-120 9.44 31 2,6-Dinitrotoluene 0.745 U 0.746 0.630 100 84.3 1 25.0-120 16.8 31 Fluoranthene 0.745 U 0.445 0.487 59.8 65.2 1 18.0-126 9.01 32 Fluorene 0.745 U 0.443 0.413 59.5 55.3 1 25.0-120 6.90 30 Hexachlorobenzene 0.745 u 0.524 0.495 70.3 66.3 1 27.0-120 5.57 28 Hexachloro-1,3-butadiene 0.745 u 0.366 0.336 49.1 45.0 1 10.0-120 8.41 38 Hexachlorocyclopentadiene 0.745 u 0.125 ND 16.8 0.000 1 10.0-120 J3 J6 200 40 Hexachloroethane 0.745 U 0.748 0.509 100 68.1 1 10.0-120 38.1 40 Indeno(1,2,3-cd)pyrene 0.745 u 0.522 0.513 70.1 68.7 1 10.0-120 1.75 32 Isophorone 0.745 U 0.978 0.767 131 103 1 13.0-120 J5 24.2 34 Naphthalene 0.745 U 0.466 0.378 62.5 50.6 1 10.0-120 20.7 35 Nitrobenzene 0.745 U 0.408 0.350 54.7 46.8 1 10.0-120 15.3 36 n-Nitrosodimethylamine 0.745 U 0.256 0.263 34.3 35.3 1 10.0-127 3.06 40 n-Nitrosodiphenylamine 0.745 U 0.575 0.471 77.1 63.1 1 17.0-120 19.8 29 n-Nitrosodi-n-propylamine 0.745 U 0.753 0.569 101 76.1 1 10.0-120 27.8 37 Phenanthrene 0.745 U 0.467 0.441 62.7 59.0 1 17.0-120 5.76 31 Benzylbutyl phthalate 0.745 U 0.463 0.554 62.2 74.2 1 23.0-120 17.9 30 Bis(2-ethylhexyl)phthalate 0.745 U 0.450 0.474 60.4 63.4 1 17.0-126 5.17 30 Di-n-butyl phthalate 0.745 U 0.379 0.486 50.9 65.0 1 30.0-120 24.7 29 Diethyl phthalate 0.745 U 0.488 0.450 65.5 60.2 1 26.0-120 8.23 28 Dimethyl phthalate 0.745 U 0.462 0.453 62.0 60.6 1 25.0-120 1.99 29 Di-n-octyl phthalate 0.745 u 0.517 0.446 69.4 59.7 1 21.0-123 14.6 29 Pyrene 0.745 0.0213 0.443 0.442 56.6 56.3 1 16.0-121 0.257 32 Pyridine 0.745 U 0.242 0.254 32.5 34.0 1 10.0-120 5.03 40 1,2,4-Trichlorobenzene 0.745 U 0.380 0.354 51.1 47.4 1 12.0-120 7.11 37 4-Chloro-3-methylphenol 0.745 U 0.631 0.569 84.8 76.1 1 15.0-120 10.4 30 2-Chlorophenol 0.745 U 0.426 0.420 57.2 56.2 1 15.0-120 1.34 37 2,4-Dichlorophenol 0.745 U 0.480 0.479 64.5 64.1 1 20.0-120 0.237 31 2,4-Dimethylphenol 0.745 U 0.572 0.513 76.8 68.7 1 10.0-120 10.9 33 4,6-Dinitro-2-methylphenol 0.745 U 0.530 0.555 71.2 74.3 1 10.0-120 4.60 39 24-Dinitrophenol 0.745 u 0.545 0.585 73.2 78.3 1 10.0-121 7.04 40 2-Nitrophenol 0.745 u 0.676 0.594 90.7 79.5 1 12.0-120 12.9 39 4-Nitrophenol 0.745 u 0.546 0.562 73.3 75.2 1 10.0-137 2.87 32 Pentachlorophenol 0.745 U 0.525 0.539 70.4 72.2 1 10.0-160 2.77 31 Phenol 0.745 U 0.483 0.471 64.8 63.1 1 12.0-120 2.38 38 2,4,5-Trichlorophenol 0.745 U 0.707 0.612 95.0 81.9 1 20.0-120 14.5 30 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: