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Geothalytical Laboratorieskc. <br />1405 Kansas Avenue Modesto CA 95351 oi— <br />epolt # P358-01 <br />Thorpe Oil <br />PO Box 357 <br />Lodi CA 95241 <br />Sample ID: TK3 @ 91 <br />Lab ID- P'202339 <br />Fax (21,-9),572-0916 <br />CERTUICATE OF ANALYSIS Date. 1/05/04 <br />Date Rec'& 12/24/03 <br />Date Started. 1/02/04 <br />Project: Ruth Marsh -3212 E, Woodson AcampoCA Date COmPleted-1/02/04 <br />Kom <br />Date Sampled: 12/24/03 <br />Time: 9,23 am <br />SaMPItr: &Azevedo(Geo) <br />Method RL <br />Analyte <br />Results Units <br />826as 510 <br />Benzene <br />2-Brorno-l-chloropropane <br />5.0 <br />Toluene <br />ND <br />5.0 <br />Ethyl Beraem <br />ND <br />5.0 <br />Total Xylenes <br />ND <br />10 <br />Methyl tern -butyl ether (MTBE) <br />Certification # 1157 <br />400 <br />Ethanol <br />ND <br />200 <br />tert-Butanol <br />'IND <br />10 <br />di-180propyl ether (WE) <br />ND <br />to <br />Ethyl text -butyl ether (ME) <br />ND <br />Cert -Amyl awffiyl eOw (TAW) <br />NI) <br />Surrogate <br />I,2-Dichloroeffiane-d4 <br />Armu$*,ed <br />20 <br />AmntRSc. %RtCO'very OCLimit % <br />22.9 114.3 66-133 <br />2-Brorno-l-chloropropane <br />20 <br />17.6 88.0 63-139 <br />4-Bromafiuorobwz ne <br />20 <br />23.0 115.0 64-136 <br />Aario D'0tbF4V, <br />Donna Keller <br />Chemist <br />Certification # 1157 <br />Laboratory Director <br />