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I Geotnalytical Laboratonies,4kc. <br />'405 Kansas Avenue Modesto, CA 95351 Phone (209) 572-M Fax (209) 572-0916 <br />"eport # P358-01 <br />CERTIFICATE OF ANALYSIS Date: 1/05/04 <br />- horpe Oil <br />Date Recld- 12/24/03 <br />PO Box 357 <br />Lodi <br />PrOject: Ruth Marsh -3212 E. woods= Acampo, CA DAde t* Stirted:1/02/04 <br />DCOPlOtthl/02/04 <br />CA 95241 <br />Ethyl Ben=w <br />ND <br />PO# Date Sampled. 12/24/03 <br />Sample ID: TKI @ 10, <br />Time: 9.40 am <br />Sampler: RAZeved0((3eo) <br />Lab TD: P202340 <br />Ntethyl Cert -butyl ether (VIISE) <br />8260B 5.0 <br />Benzene <br />ND rig/Kg <br />5k <br />Toluene <br />ND <br />5X <br />Ethyl Ben=w <br />ND <br />5.0 <br />Total Xylenes <br />ND <br />10 <br />Ntethyl Cert -butyl ether (VIISE) <br />ND <br />400 <br />Ethanol <br />ND <br />200 <br />tert-Butanol <br />ND <br />10 <br />di -isopropyl ether (DIPE) <br />ND <br />10 <br />Ethyl tert-butyl ether (ME) <br />10 <br />tert-Amyl mmthyi ether (TANIE) <br />ND <br />Surrogate <br />1,2-Dichloroethane-d, <br />Arnnt *ked <br />20 <br />Arnm Ree. % Recovery <)C Lmt % <br />23.5 1175 66-133 <br />2-Brorno-1-chloropropane <br />20 <br />19.6 98.0 63-139 <br />ario U�alo <br />Chemist <br />4-Bromoiliwrobenzene <br />Certification #'1157 <br />20 <br />22.4 112,0 64-136 <br />Donna Keller <br />Laboratory Director <br />