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WG1517013 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1244020-01 ONE LAB. NATIONWIDE. 40 L1243747-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1243747-09 07/29/20 14:30 • (MS) R3554385-3 07/29/20 18:08 (MSD) R3554385-4 07/29/20 18:28 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/1 mg/I mg/I mg/I % % % % % Bromomethane 0.00500 ND ND ND 23.4 34.4 1 10.0-160 J3 38.1 38 n-Butylbenzene 0.00500 ND 0.00405 0.00377 81.0 75.4 1 31.0-150 7.16 30 sec-Butylbenzene 0.00500 ND 0.00438 0.00403 87.6 80.6 1 33.0-155 8.32 29 tert-Butylbenzene 0.00500 ND 0.00433 0.00414 86.6 82.8 1 34.0-153 4.49 28 Carbon tetrachloride 0.00500 ND 0.00507 0.00480 101 96.0 1 23.0-159 5.47 28 Chlorobenzene 0.00500 ND 0.00481 0.00435 96.2 87.0 1 33.0-152 10.0 27 Chlorodibromomethane 0.00500 ND 0.00496 0.00449 99.2 89.8 1 37.0-149 9.95 27 Chloroethane 0.00500 ND ND ND 58.4 52.6 1 10.0-160 10.5 30 Chloroform 0.00500 ND ND ND 87.6 86.6 1 29.0-154 1.01 28 Chloromethane 0.00500 ND 0.00265 0.00311 53.0 62.2 1 10.0-160 16.0 29 Acrolein 0.0250 ND 0.0584 0.0567 234 227 1 10.0-160 J5 J5 2.95 39 1,2-Dibromo-3-Chloropropane 0.00500 ND ND ND 95.8 93.8 1 22.0-151 2.11 34 1,2-Dibromoethane 0.00500 ND 0.00481 0.00445 96.2 89.0 1 34.0-147 7.78 27 Dibromomethane 0.00500 ND 0.00465 0.00458 93.0 91.6 1 30.0-151 1.52 27 1,2-Dichlorobenzene 0.00500 ND 0.00460 0.00424 92.0 84.8 1 34.0-149 8.14 28 1,3-Dichlorobenzene 0.00500 ND 0.00441 0.00417 88.2 83.4 1 36.0-146 5.59 27 14-Dichlorobenzene 0.00500 ND 0.00445 0.00414 89.0 82.8 1 35.0-142 7.22 27 Dichlorodifluoromethane 0.00500 ND 0.00601 0.00581 120 116 1 10.0-160 3.38 29 1,1-Dichloroethane 0.00500 ND 0.00498 0.00468 92.5 86.5 1 25.0-158 6.21 27 1,2-Dichloroethane 0.00500 ND 0.00409 0.00405 81.8 81.0 1 29.0-151 0.983 27 1,1-Dichloroethene 0.00500 0.00947 0.0143 0.0138 96.6 86.6 1 11.0-160 3.56 29 cis-1,2-Dichloroethene 0.00500 0.00398 0.00868 0.00875 94.0 95.4 1 10.0-160 0.803 27 trans-1,2-Dichloroethene 0.00500 ND 0.00516 0.00469 96.5 87.1 1 17.0-153 9.54 27 1,2-Dichloropropane 0.00500 ND 0.00456 0.00453 91.2 90.6 1 30.0-156 0.660 27 2-Chloroethyl vinyl ether 0.0250 ND ND ND 0.000 0.000 1 10.0-160 J6 J6 0.000 31 cis-1,3-Dichloropropene 0.00500 ND 0.00417 0.00401 83.4 80.2 1 34.0-149 3.91 28 trans-1,3-Dichloropropene 0.00500 ND 0.00388 0.00369 77.6 73.8 1 32.0-149 5.02 28 2-Chlorotoluene 0.00500 ND 0.00431 0.00395 86.2 79.0 1 32.0-153 8.72 28 4-Chlorotoluene 0.00500 ND 0.00417 0.00397 83.4 79.4 1 32.0-150 4.91 28 Di-isopropyl ether 0.00500 ND 0.00456 0.00427 91.2 85.4 1 21.0-160 6.57 28 Ethylbenzene 0.00500 ND 0.00473 0.00425 94.6 85.0 1 30.0-155 10.7 27 Hexachloro-1,3-butadiene 0.00500 ND 0.00506 0.00474 101 94.8 1 20.0-154 6.53 34 Isopropylbenzene 0.00500 ND 0.00459 0.00422 91.8 84.4 1 28.0-157 8.40 27 p-Isopropyltoluene 0.00500 ND 0.00449 0.00422 89.8 84.4 1 30.0-154 6.20 29 2-Butanone (MEK) 0.0250 ND 0.0175 0.0187 70.0 74.8 1 10.0-160 6.63 32 Methylene Chloride 0.00500 ND ND ND 92.4 84.8 1 23.0-144 8.58 28 4-Methyl-2-pentanone (MIBK) 0.0250 ND 0.0191 0.0191 76.4 76.4 1 29.0-160 0.000 29 Methyl tert-butyl ether 0.00500 ND 0.00437 0.00440 87.4 88.0 1 28.0-150 0.684 29 1,1-Dichloropropene 0.00500 ND 0.00466 0.00423 93.2 84.6 1 25.0-158 9.67 27 Naphthalene 0.00500 ND ND ND 86.2 85.8 1 12.0-156 0.465 35 6 Qc 4 Cn 3 SS Cp 2 Tc 9 Sc GI Al ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Carolina Casualty Ins. Co. 016273 L1244020 08/03/201416 20 of 31