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WG1517013 QUALITY CONTROL SUMMARY <br />4 <br />Cn <br />2 <br />Tc <br />3 <br />SS <br />9 <br />SC <br />GI <br />Al <br />ONE LAB. NATIONWIDE. 410 <br />Volatile Organic Compounds (GC/MS) by Method 82606 L1244020-01 <br />L1243747-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) <br />(OS) L1243747-09 07/29/20 14:30 • (MS) R3554385-3 07/29/20 18:08 • (MSD) R3554385-4 07/29/20 18:28 <br />Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits <br />Analyte mg/I mg/I mg/I mg/I % % % % % <br />1,3-Dichloropropane 0.00500 ND 0.00465 0.00447 93.0 89.4 1 38.0-147 3.95 27 <br />n-Propylbenzene 0.00500 ND 0.00407 0.00396 81.4 79.2 1 31.0-154 2.74 28 <br />Styrene 0.00500 ND 0.00388 0.00364 77.6 72.8 1 33.0-155 6.38 28 <br />1,1,1,2-Tetrachloroethane 0.00500 ND 0.00490 0.00452 98.0 90.4 1 36.0-151 8.07 29 <br />2,2-Dichloropropane 0.00500 ND 0.00419 0.00387 83.8 77.4 1 24.0-152 7.94 29 <br />1,1,2,2-Tetrachloroethane 0.00500 ND 0.00451 0.00436 90.2 87.2 1 33.0-150 3.38 28 <br />Tetrachloroethene 0.00500 0.00167 0.00702 0.00660 107 98.6 1 10.0-160 6.17 27 <br />Toluene 0.00500 ND 0.00439 0.00414 87.8 82.8 1 26.0-154 5.86 28 <br />1,1,2-Trichlorotrifluoroethane 0.00500 0.0165 0.0187 0.0194 44.0 58.0 1 23.0-160 3.67 30 <br />1,2,4-Trichlorobenzene 0.00500 ND 0.00449 0.00468 89.8 93.6 1 24.0-150 4.14 33 <br />1,1,1-Trichloroethane 0.00500 ND 0.00529 0.00472 106 94.4 1 23.0-160 11.4 28 <br />1,1,2-Trichloroethane 0.00500 ND 0.00515 0.00483 103 96.6 1 35.0-147 6.41 27 <br />Trichloroethene 0.00500 0.110 0.110 0.110 0.000 0.000 1 10.0-160 V V 0.000 25 <br />Trichlorofluoromethane 0.00500 ND ND ND 80.6 74.4 1 17.0-160 7.64 31 <br />1,2,3-Trichloropropane 0.00500 ND 0.00458 0.00454 91.6 90.8 1 34.0-151 0.877 29 <br />1,2,4-Trimethylbenzene 0.00500 ND 0.00429 0.00404 85.8 80.8 1 26.0-154 6.00 27 <br />1,3,5-Trimethylbenzene 0.00500 ND 0.00427 0.00398 85.4 79.6 1 28.0-153 7.03 27 <br />Vinyl chloride 0.00500 ND 0.00356 0.00322 71.2 64.4 1 10.0-160 10.0 27 <br />Xylenes, Total 0.0150 ND 0.0138 0.0125 92.0 83.3 1 29.0-154 9.89 28 <br />1,2,3-Trichlorobenzene 0.00500 ND 0.00449 0.00466 89.8 93.2 1 17.0-150 3.72 36 <br />1,2,3-Trimethylbenzene 0.00500 ND 0.00430 0.00392 86.0 78.4 1 32.0-149 9.25 28 <br />(S) Toluene-d8 90.6 88.2 80.0-120 <br />(S) 4-Bromofluorobenzene 96.8 94.8 77.0-126 <br />(S)1,2-Dichloroethane-d4 78.8 83.7 70.0-130 <br />L1243748-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) <br />(OS) L1243748-03 07/29/20 15:49 • (MS) R3554385-5 07/29/20 18:48 • (MSD) R3554385-6 07/29/20 19:08 <br />Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits <br />Analyte mg/I mg/I mg/I mg/I % % % % % <br />Acetone 0.0250 ND ND ND 81.2 82.0 1 10.0-160 0.980 35 <br />Acrylonitrile 0.0250 ND 0.0226 0.0230 90.4 92.0 1 21.0-160 1.75 32 <br />Benzene 0.00500 ND 0.00543 0.00533 109 107 1 17.0-158 1.86 27 <br />Bromobenzene 0.00500 ND 0.00425 0.00427 85.0 85.4 1 30.0-149 0.469 28 <br />Bromodichloromethane 0.00500 ND 0.00514 0.00483 103 96.6 1 31.0-150 6.22 27 <br />Bromoform 0.00500 ND 0.00505 0.00485 101 97.0 1 29.0-150 4.04 29 <br />Bromomethane 0.00500 ND ND ND 43.6 43.4 1 10.0-160 0.460 38 <br />n-Butylbenzene 0.00500 ND 0.00401 0.00419 80.2 83.8 1 31.0-150 4.39 30 <br />sec-Butylbenzene 0.00500 ND 0.00467 0.00454 93.4 90.8 1 33.0-155 2.82 29 <br />ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br />Carolina Casualty Ins. Co. 016273 L1244020 08/03/2014:16 21 of 31 <br />p <br />6 <br />Oc