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McCampbell Analytical, Inc. <br />witat "When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com <br /> <br />Analytical Report <br />Client: Yara North America WorkOrder: 2101638 <br />Date Received: 01/14/2021 14:17 <br />Extraction Method: SW5030B <br />Date Prepared: 01/14/2021 Analytical Method: 5W8260B <br />Project: New Site Pond <br /> <br />Unit: mg/kg <br />Volatile Organics <br />Client ID Lab ID Matrix Date Collected Instrument Batch II) <br />Pond Center 2101638-001A Soil 01/14/2021 10:00 GC16 01152109.D 213160 <br />Analytes Result EL <br />0.0050 <br />DF <br />1 <br />Date Analyzed <br />1,1-Dichloropropene ND 01/15/2021 11:50 <br />cis-1,3-Dichloropropene ND 0.0050 1 01/15/2021 11:50 <br />trans-1,3-Dichloropropene ND 0.0050 1 01/15/2021 11:50 <br />Diisopropyl ether (DIPE) ND 0.0050 1 01/15/2021 11:50 <br />Ethylbenzene ND 0.0050 1 01/15/2021 11:50 <br />Ethyl tert-butyl ether (ETBE) ND 0.0050 1 01/15/2021 11:50 <br />Freon 113 ND 0.0050 1 01/15/2021 11:50 <br />Hexachlorobutadiene ND 0.0050 1 01/15/2021 11:50 <br />Hexachloroethane ND 0.0050 1 01/15/2021 11:50 <br />2-Hexanone ND 0.0050 1 01/15/2021 11:50 <br />Isopropylbenzene ND 0.0050 1 01/15/2021 11:50 <br />4-Isopropyl toluene ND 0.0050 1 01/15/2021 11:50 <br />Methyl-t-butyl ether (MTBE) ND 0.0050 1 01/15/2021 11:50 <br />Methylene chloride ND 0.020 1 01/15/2021 11:50 <br />4-Methyl-2-pentanone (MIBK) ND 0.0050 1 01/15/2021 11:50 <br />Naphthalene ND 0.0050 1 01/15/2021 11:50 <br />n-Propyl benzene ND 0.0050 1 01/15/2021 11:50 <br />Styrene ND 0.0050 1 01/15/2021 11:50 <br />1,1,1,2-Tetrachloroethane ND 0.0050 1 01/15/2021 11:50 <br />1,1,2,2-Tetrachloroethane ND 0.0050 1 01/15/2021 11:50 <br />Tetrachloroethene ND 0.0050 1 01/15/2021 11:50 <br />Toluene ND 0.0050 1 01/15/2021 11:50 <br />1,2,3-Trichlorobenzene ND 0.0050 1 01/15/2021 11:50 <br />1,2,4-Trichlorobenzene ND 0.0050 1 01/15/2021 11:50 <br />1,1,1-Trichloroethane ND 0.0050 1 01/15/2021 11:50 <br />1,1,2-Trichloroethane ND 0.0050 1 01/15/2021 11:50 <br />Trichloroethene ND 0.0050 1 01/15/2021 11:50 <br />Trichlorofluoromethane ND 0.0050 1 01/15/2021 11:50 <br />1,2,3-Trichloropropane ND 0.0050 1 01/15/2021 11:50 <br />1,2,4-Trimethylbenzene ND 0.0050 1 01/15/2021 11:50 <br />1,3,5-Trimethylbenzene ND 0.0050 1 01/15/2021 11:50 <br />Vinyl Chloride ND 0.0050 1 01/15/2021 11:50 <br />m,p-Xylene ND 0.0050 1 01/15/2021 11:50 <br />o-Xylene ND 0.0050 1 01/15/2021 11:50 <br />Xylenes, Total ND 0.0050 1 01/15/2021 11:50 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 5 of 51