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McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877)252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com <br /> <br />Analytical Report <br />Client: Yara North America WorkOrder: 2101638 <br />Date Received: 01/14/2021 14:17 <br />Extraction Method: SW5030B <br />Date Prepared: 01/14/2021 Analytical Method: SW8260B <br />Project: New Site Pond <br /> <br />Unit: mg/kg <br />Volatile Organics <br />Client ID <br />La I) ID <br /> <br />Matrix Date Collected Instrument Batch ID <br />Pond Center <br />2101638-001A Soil <br /> 01/14/2021 10:00 GC16 01162109.D <br />213160 <br />Analytes Result RL DF Date Analyzed <br /> <br />Surrogates REC (%) Limits <br />Dibromofluoromethane 88 70-140 01/15/2021 11:50 <br />Toluene-d8 106 70-140 01/15/2021 11:50 <br />4-BFB 101 70-140 01/15/2021 11:50 <br />Benzene-d6 74 50-140 01/15/2021 11:50 <br />Ethylbenzene-d10 93 50-140 01/15/2021 11:50 <br />1,2-DCB-d4 71 40-140 01/15/2021 11:50 <br />Analyst(s): KF <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 6 of 51