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McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com <br /> <br />Analytical Report <br />Client: Yara North America Work0 rder: 2101638 <br />Date Received: 01/14/2021 14:17 <br />Extraction Method: SW5030B <br />Date Prepared: 01/14/2021 <br /> <br />Analytical Method: SW8260B <br />Project: New Site Pond <br /> <br />Unit: mg/kg <br />Volatile Organics <br />Client ID Lab ID Matrix Date Collected Instrument Batch ID <br />Pond Edge 2101638-002A Soil 01/14/2021 10:00 GC16 01152110.D 213160 <br />Analytes Result RL <br />0.20 <br />DF <br />1 <br />Date Analyzed <br />Acetone ND 01/15/2021 12:30 <br />tert-Amyl methyl ether (TAME) ND 0.0050 1 01/15/2021 12:30 <br />Benzene ND 0.0050 1 01/15/2021 12:30 <br />Bromobenzene ND 0.0050 1 01/15/2021 12:30 <br />Bromochloromethane ND 0.0050 1 01/15/2021 12:30 <br />Bromodichloromethane ND 0.0050 1 01/15/2021 12:30 <br />Bromoform ND 0.0050 1 01/15/2021 12:30 <br />Bromomethane ND 0.0050 1 01/15/2021 12:30 <br />2-Butanone (MEK) ND 0.050 1 01/15/2021 12:30 <br />t-Butyl alcohol (TBA) ND 0.050 1 01/15/2021 12:30 <br />n-Butyl benzene ND 0.0050 1 01/15/2021 12:30 <br />sec-Butyl benzene ND 0.0050 1 01/15/2021 12:30 <br />tert-Butyl benzene ND 0.0050 1 01/15/2021 12:30 <br />Carbon Disulfide ND 0.0050 1 01/15/2021 12:30 <br />Carbon Tetrachloride ND 0.0050 1 01/15/2021 12:30 <br />Chlorobenzene ND 0.0050 1 01/15/2021 12:30 <br />Chloroethane ND 0.0050 1 01/15/2021 12:30 <br />Chloroform ND 0.0050 1 01/15/2021 12:30 <br />Chloromethane ND 0.0050 1 01/15/2021 12:30 <br />2-Chlorotoluene ND 0.0050 1 01/15/2021 12:30 <br />4-Chlorotoluene ND 0.0050 1 01/15/2021 12:30 <br />Dibromochloromethane ND 0.0050 1 01/15/2021 12:30 <br />1,2-Dibromo-3-chloropropane ND 0.0050 1 01/15/2021 12:30 <br />1,2-Dibromoethane (EDB) ND 0.0050 1 01/15/2021 12:30 <br />Dibromomethane ND 0.0050 1 01/15/2021 12:30 <br />1,2-Dichlorobenzene ND 0.0050 1 01/15/2021 12:30 <br />1,3-Dichlorobenzene ND 0.0050 1 01/15/2021 12:30 <br />1,4-Dichlorobenzene ND 0.0050 1 01/15/2021 12:30 <br />Dichlorodifluoromethane ND 0.0050 1 01/15/2021 12:30 <br />1,1-Dichloroethane ND 0.0050 1 01/15/2021 12:30 <br />1,2-Dichloroethane (1,2-DCA) ND 0.0050 1 01/15/2021 12:30 <br />1,1-Dichloroethene ND 0.0050 1 01/15/2021 12:30 <br />cis-1,2-Dichloroethene ND 0.0050 1 01/15/2021 12:30 <br />trans-1,2-Dichloroethene ND 0.0050 1 01/15/2021 12:30 <br />1,2-Dichloropropane ND 0.0050 1 01/15/2021 12:30 <br />1,3-Dichloropropane ND 0.0050 1 01/15/2021 12:30 <br />2,2-Dichloropropane ND 0.0050 1 01/15/2021 12:30 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 7 of 51