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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-001-MB Date Extracted: 04-17-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: Method Blank Date Received: NA GC Column: DB5MS 2005 WHO TEQ: 0.0
<br />Matrix: Solid Amount: 5.00 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4475
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.162 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.199 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.283 -0.0793
<br />1,2,3,6,7,8-HxCDD ND 0.287 -0.0940 Total TCDD ND 0.162
<br />1,2,3,7,8,9-HxCDD ND 0.261 -0.0823 Total PeCDD ND 0.199
<br />1,2,3,4,6,7,8-HpCDD ND 0.328 -0.0842 Total HxCDD ND 0.287
<br />OCDD ND 0.708 - 0.172 Total HpCDD ND 0.328
<br />2,3,7,8-TCDF ND 0.110 -0.0269
<br />1,2,3,7,8-PeCDF ND 0.171 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.172 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.261 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.256 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.276 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.309 -0.0657 Total TCDF ND 0.110
<br />1,2,3,4,6,7,8-HpCDF ND 0.314 -0.0747 Total PeCDF ND 0.172
<br />1,2,3,4,7,8,9-HpCDF ND 0.358 -0.0883 Total HxCDF ND 0.309
<br />OCDF ND 0.688 -0.170 Total HpCDF ND 0.358
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 96.4 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 97.4 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 102 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 102 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 89.7 23.0 - 140
<br />13C-OCDD 72.0 17.0 - 157
<br />13C-2,3,7,8-TCDF 95.4 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 93.3 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 92.9 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 93.8 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 91.1 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 90.3 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 88.1 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 90.6 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 90.5 26.0 - 138
<br />13C-OCDF 75.8 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 89.1 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/19/2018 4/19/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />000005 of 000033
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