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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-013-SA Date Extracted: 04-17-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-13 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 2.89
<br />Matrix: Solid Amount: 5.05 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4475 % Solids: 94.87
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.170 - 0.0273
<br />1,2,3,7,8-PeCDD 0.663 - J 0.663 0.0570
<br />1,2,3,4,7,8-HxCDD 0.877 - J 0.0877 0.0793
<br />1,2,3,6,7,8-HxCDD 2.60 - J 0.260 0.0940 Total TCDD ND 0.170
<br />1,2,3,7,8,9-HxCDD 1.45 - J 0.145 0.0823 Total PeCDD 2.30 -J
<br />1,2,3,4,6,7,8-HpCDD 71.3 -0.713 0.0842 Total HxCDD 18.8 -
<br />OCDD 629 -0.189 0.172 Total HpCDD 128 -
<br />2,3,7,8-TCDF 1.22 -0.122 0.0269
<br />1,2,3,7,8-PeCDF 0.397 - J 0.0119 0.0449
<br />2,3,4,7,8-PeCDF 0.927 - J 0.278 0.0468
<br />1,2,3,4,7,8-HxCDF 0.913 - J 0.0913 0.0437
<br />1,2,3,6,7,8-HxCDF 0.845 - J 0.0845 0.0417
<br />2,3,4,6,7,8-HxCDF 1.03 - J 0.103 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.233 -0.0657 Total TCDF 6.98 -
<br />1,2,3,4,6,7,8-HpCDF 12.5 -0.125 0.0747 Total PeCDF 8.44 -
<br />1,2,3,4,7,8,9-HpCDF 0.901 - J 0.00901 0.0883 Total HxCDF 16.6 -
<br />OCDF 37.1 -0.0111 0.170 Total HpCDF 36.9 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 96.7 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 99.1 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 100 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 99.6 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 87.4 23.0 - 140
<br />13C-OCDD 75.2 17.0 - 157
<br />13C-2,3,7,8-TCDF 98.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 97.5 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 96.5 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 93.8 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 90.9 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 88.3 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 85.6 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 88.6 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 89.4 26.0 - 138
<br />13C-OCDF 76.8 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 91.8 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/19/2018 4/19/2018
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