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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-012-SA Date Extracted: 04-17-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-12 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 1.08
<br />Matrix: Solid Amount: 5.05 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4475 % Solids: 96.77
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.174 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.318 -0.0570
<br />1,2,3,4,7,8-HxCDD 0.494 - J 0.0494 0.0793
<br />1,2,3,6,7,8-HxCDD 1.73 - J 0.173 0.0940 Total TCDD ND 0.174
<br />1,2,3,7,8,9-HxCDD 1.06 - J 0.106 0.0823 Total PeCDD ND 0.318
<br />1,2,3,4,6,7,8-HpCDD 33.3 -0.333 0.0842 Total HxCDD 11.1 -
<br />OCDD 302 -0.0906 0.172 Total HpCDD 61.2 -
<br />2,3,7,8-TCDF 0.699 - J 0.0699 0.0269
<br />1,2,3,7,8-PeCDF ND 0.200 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.205 -0.0468
<br />1,2,3,4,7,8-HxCDF 0.621 - J 0.0621 0.0437
<br />1,2,3,6,7,8-HxCDF 0.522 - J 0.0522 0.0417
<br />2,3,4,6,7,8-HxCDF 0.673 - J 0.0673 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.144 -0.0657 Total TCDF 3.68 -
<br />1,2,3,4,6,7,8-HpCDF 6.91 -0.0691 0.0747 Total PeCDF 3.76 -J
<br />1,2,3,4,7,8,9-HpCDF 0.576 - J 0.00576 0.0883 Total HxCDF 10.0 -
<br />OCDF 21.2 -0.00636 0.170 Total HpCDF 19.4 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 95.7 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 102 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 99.8 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 98.0 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 90.0 23.0 - 140
<br />13C-OCDD 73.3 17.0 - 157
<br />13C-2,3,7,8-TCDF 96.8 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 97.2 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 97.8 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 91.9 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 86.5 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 84.6 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 86.9 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 87.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 90.6 26.0 - 138
<br />13C-OCDF 76.7 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 85.9 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/19/2018 4/19/2018
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