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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11471-004-SA Date Extracted: 04-30-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: VS59 Date Received: 04-13-2018 GC Column: DB5MS 2005 WHO TEQ: 0.332
<br />Matrix: Soil Amount: 5.02 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4493 % Solids: 93.03
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.154 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.260 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.323 -0.0793
<br />1,2,3,6,7,8-HxCDD ND 0.351 -0.0940 Total TCDD 0.433 -J
<br />1,2,3,7,8,9-HxCDD ND 0.308 -0.0823 Total PeCDD ND 0.260
<br />1,2,3,4,6,7,8-HpCDD 3.03 - J 0.0303 0.0842 Total HxCDD ND 0.351
<br />OCDD 31.5 -0.00945 0.172 Total HpCDD 5.92 -
<br />2,3,7,8-TCDF ND 0.197 -0.0269
<br />1,2,3,7,8-PeCDF ND 0.167 -0.0449
<br />2,3,4,7,8-PeCDF 0.952 - J 0.286 0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.157 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.157 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.163 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.205 -0.0657 Total TCDF 1.37 -M
<br />1,2,3,4,6,7,8-HpCDF 0.586 - J 0.00586 0.0747 Total PeCDF 5.22 -
<br />1,2,3,4,7,8,9-HpCDF ND 0.139 -0.0883 Total HxCDF 1.02 -J
<br />OCDF 3.44 - J 0.00103 0.170 Total HpCDF 2.28 -J
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 80.5 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 88.1 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 106 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 102 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 87.8 23.0 - 140
<br />13C-OCDD 82.7 17.0 - 157
<br />13C-2,3,7,8-TCDF 80.7 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 91.6 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 92.0 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 96.5 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 93.0 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 90.5 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 83.4 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 78.4 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 81.6 26.0 - 138
<br />13C-OCDF 79.4 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 74.8 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/2/2018 5/2/2018
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