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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11471-005-SA Date Extracted: 04-30-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: VS65 Date Received: 04-13-2018 GC Column: DB5MS 2005 WHO TEQ: 0.139
<br />Matrix: Soil Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4493 % Solids: 95.58
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.184 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.232 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.222 -0.0793
<br />1,2,3,6,7,8-HxCDD ND 0.239 -0.0940 Total TCDD ND 0.184
<br />1,2,3,7,8,9-HxCDD ND 0.211 -0.0823 Total PeCDD ND 0.232
<br />1,2,3,4,6,7,8-HpCDD 5.37 -0.0537 0.0842 Total HxCDD 2.20 -J
<br />OCDD 52.8 -0.0158 0.172 Total HpCDD 10.2 -
<br />2,3,7,8-TCDF 0.561 - J 0.0561 0.0269
<br />1,2,3,7,8-PeCDF ND 0.131 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.140 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.131 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.139 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.148 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.194 -0.0657 Total TCDF 1.91 -
<br />1,2,3,4,6,7,8-HpCDF 1.18 - J 0.0118 0.0747 Total PeCDF 0.776 -J
<br />1,2,3,4,7,8,9-HpCDF ND 0.143 -0.0883 Total HxCDF 1.20 -J
<br />OCDF 4.63 - J 0.00139 0.170 Total HpCDF 4.03 -J
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 78.2 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 86.3 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 107 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 100 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 88.8 23.0 - 140
<br />13C-OCDD 86.0 17.0 - 157
<br />13C-2,3,7,8-TCDF 77.8 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 91.3 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 91.2 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 95.1 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 92.6 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 89.5 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 78.6 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 78.8 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 74.4 26.0 - 138
<br />13C-OCDF 82.5 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 69.2 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/2/2018 5/2/2018
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