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USED OIL RAGS/PPE DEBRIS B SAMPLE RESULTS - 01 Collected date/time: 03/15/21 13:00 L1328467 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/kg mg/kg mg/kg date/time Bromodichloromethane U 0.0145 0.0500 20 03/22/202106:53 WG1638308 FTc Bromoform U 0.0234 0.500 20 03/22/202106:53 WG1638308 Bromomethane U 0.0394 0.250 20 03/22/202106:53 WG1638308 FSS n-Butylbenzene 0.687 0.105 0.250 20 03/22/202106:53 WG1638308 sec-Butyl benzene 0.406 0.0576 0.250 20 03/22/202106:53 WG1638308 tert-Butylbenzene U 0.0390 0.100 20 03/22/202106:53 WG1638308 4 Cn Carbon tetrachloride U 0.0180 0.100 20 03/22/202106:53 WG1638308 Chlorobenzene U 0.00420 0.0500 20 03/22/202106:53 WG1638308 Chlorodibromomethane U 0.0122 0.0500 20 03/22/202106:53 WG1638308 Chloroethane U 0.0340 0.100 20 03/22/202106:53 WG1638308 Chloroform U 0.0206 0.0500 20 03/22/202106:53 WG1638308 Rc Chloromethane U 0.0870 0.250 20 03/22/202106:53 WG1638308 2-Chlorotoluene U 0.0173 0.0500 20 03/22/202106:53 WG1638308 4-Chlorotoluene U 0.00900 0.100 20 03/22/202106:53 WG1638308 GI 1,2-Dibromo-3-Chloropropane U 0.0780 0.500 20 03/22/202106:53 WG1638308 1,2-Dibromoethane U 0.0130 0.0500 20 03/22/202106:53 WG1638308 FAI Dibromomethane U 0.0150 0.100 20 03/22/202106:53 WG1638308 1,2-Dichlorobenzene U 0.00850 0.100 20 03/22/202106:53 WG1638308 FSC 1,3-Dichlorobenzene U 0.0120 0.100 20 03/22/202106:53 WG1638308 1,4-Dichlorobenzene U 0.0140 0.100 20 03/22/202106:53 WG1638308 Dichlorodifluoromethane U 0.0322 0.0500 20 03/22/202106:53 WG1638308 1,1-Dichloroethane U 0.00982 0.0500 20 03/22/202106:53 WG1638308 1,2-Dichloroethane U 0.0130 0.0500 20 03/22/202106:53 WG1638308 1,1-Dichloroethene U 0.0121 0.0500 20 03/22/202106:53 WG1638308 cis-1,2-Dichloroethene U 0.0147 0.0500 20 03/22/202106:53 WG1638308 trans-1,2-Dichloroethene U 0.0208 0.100 20 03/22/202106:53 WG1638308 1,2-Dichloropropane U 0.0284 0.100 20 03/22/202106:53 WG1638308 1,1-Dichloropropene U 0.0162 0.0500 20 03/22/202106:53 WG1638308 1,3-Dichloropropane U 0.0100 0.100 20 03/22/202106:53 WG1638308 cis-1,3-Dichloropropene U 0.0151 0.0500 20 03/22/202106:53 WG1638308 trans-1,3-Dichloropropene U 0.0228 0.100 20 03/22/202106:53 WG1638308 2,2-Dichloropropane U 0.0276 0.0500 20 03/22/202106:53 WG1638308 Di-isopropyl ether U 0.00820 0.0200 20 03/22/202106:53 WG1638308 Ethylbenzene 0.893 0.0147 0.0500 20 03/22/202106:53 WG1638308 Hexachloro-1,3-butadiene U 0.120 0.500 20 03/22/202106:53 WG1638308 Isopropylbenzene 0.247 0.00850 0.0500 20 03/22/202106:53 WG1638308 p-Isopropyltoluene 0.273 0.0510 0.100 20 03/22/202106:53 WG1638308 2-Butanone(MEK) U 1.27 2.00 20 03/22/202106:53 WG1638308 Methylene Chloride U 0.133 0.500 20 03/22/202106:53 WG1638308 4-Methyl-2-pentanone(MIBK) U 0.0456 0.500 20 03/22/202106:53 WG1638308 Methyl tert-butyl ether U 0.00700 0.0200 20 03/22/202106:53 WG1638308 Naphthalene 0.215 J 0.0976 0.250 20 03/22/202106:53 WG1638308 n-Propylbenzene 1.18 0.0190 0.100 20 03/22/202106:53 WG1638308 Styrene U 0.00458 0.250 20 03/22/202106:53 WG1638308 1,1,1,2-Tetrachloroethane U 0.0190 0.0500 20 03/22/202106:53 WG1638308 1,1,2,2-Tetrachloroethane U 0.0139 0.0500 20 03/22/202106:53 WG1638308 1,1,2-Trichlorotrifluoroethane U 0.0151 0.0500 20 03/22/202106:53 WG1638308 Tetrachloroethene U 0.0179 0.0500 20 03/22/202106:53 WG1638308 Toluene 0.480 0.0260 0.100 20 03/22/202106:53 WG1638308 1,2,3-Trichlorobenzene U 0.147 0.250 20 03/22/202106:53 WG1638308 1,2,4-Trichlorobenzene U 0.0880 0.250 20 03/22/202106:53 WG1638308 1,1,1-Trichloroethane U 0.0185 0.0500 20 03/22/202106:53 WG1638308 1,1,2-Trichloroethane U 0.0119 0.0500 20 03/22/202106:53 WG1638308 Trichloroethene U 0.0117 0.0200 20 03/22/202106:53 WG1638308 Trichlorofluoromethane U 0.0165 0.0500 20 03/22/202106:53 WG1638308 1,2,3-Trichloropropane U 0.0324 0.250 20 03/22/202106:53 WG1638308 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 6 of32