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USED OIL RAGS/PPE DEBRIS B SAMPLE RESULTS - 01 <br /> Collected date/time: 03/15/21 13:00 L1328467 <br /> Volatile Organic Compounds (GC/MS) by Method 82608 <br /> Result Qualifier MDL RDL Dilution Analysis Batch Cp <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> 1,2,4-Trimethyl benzene 5.85 0.0316 0.100 20 03/22/202106:53 WG1638308 FTc <br /> 1,2,3-Trimethyl benzene 1.72 0.0316 0.100 20 03/22/202106:53 WG1638308 <br /> 1,3,5-Trimethyl benzene 1.62 0.0400 0.100 20 03/22/202106:53 WG1638308 FSS <br /> Vinyl chloride U 0.0232 0.0500 20 03/22/202106:53 WG1638308 <br /> Xylenes,Total 5.29 0.0176 0.130 20 03/22/202106:53 WG1638308 <br /> (S)Toluene-d8 110 75.0-131 03/22/202106:53 WG1638308 4Cn <br /> (S)4-Bromofluorobenzene 93.9 67.0-138 03/22/202106:53 WG1638308 <br /> (S)1,2-Dich/oroethone-d4 100 70.0-130 03/22/202106:53 WG1638308 <br /> Sample Narrative: <br /> L1328467-01 WG1638308:Non-target compounds too high to run at a lower dilution. Rc <br /> Semi-Volatile Organic Compounds (GC) by Method 8015AGI <br /> Result Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time FAI C12-C22 Hydrocarbons 29800 2140 11700 2920 03/26/202101:55 WG1639779 <br /> C22-02 Hydrocarbons 83500 3880 11700 2920 03/26/202101:55 WG1639779 <br /> C32-C40 Hydrocarbons 65500 3880 11700 2920 03/26/202101:55 WG1639779 FSC <br /> (S)o-Terpheny/ 0.000 J7 18.0-148 03/26/202101:55 WG1639779 <br /> Semi Volatile Organic Compounds (GC/MS) by Method 8270C <br /> Result Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> Acenaphthene U 0.787 4.86 146 03/25/202100:58 WG1639121 <br /> Acenaphthylene U 0.685 4.86 146 03/25/202100:58 WG1639121 <br /> Anthracene U 0.866 4.86 146 03/25/202100:58 WG1639121 <br /> Benzidine U 9.14 244 146 03/25/202100:58 WG1639121 <br /> Benzo(a)anthracene U 0.857 4.86 146 03/25/202100:58 WG1639121 <br /> Benzo(b)fluoranthene U 0.907 4.86 146 03/25/202100:58 WG1639121 <br /> Benzo(k)fluoranthene U 0.864 4.86 146 03/25/202100:58 WG1639121 <br /> Benzo(g,h,i)perylene U 0.889 4.86 146 03/25/202100:58 WG1639121 <br /> Benzo(a)pyrene U 0.904 4.86 146 03/25/202100:58 WG1639121 <br /> Bis(2-chlorethoxy)methane U 1.46 48.6 146 03/25/202100:58 WG1639121 <br /> Bis(2-chloroethyl)ether U 1.61 48.6 146 03/25/202100:58 WG1639121 <br /> 2,2-Oxybis(1-Chloropropane) U 2.10 48.6 146 03/25/202100:58 WG1639121 <br /> 4-Bromophenyl-phenylether U 1.71 48.6 146 03/25/202100:58 WG1639121 <br /> 2-Chloronaphthalene U 0.854 4.86 146 03/25/202100:58 WG1639121 <br /> 4-Chlorophenyl-phenylether U 1.69 48.6 146 03/25/202100:58 WG1639121 <br /> Chrysene U 0.967 4.86 146 03/25/202100:58 WG1639121 <br /> Dibenz(a,h)anthracene U 1.35 4.86 146 03/25/202100:58 WG1639121 <br /> 3,3-Dichlorobenzidine U 1.80 48.6 146 03/25/202100:58 WG1639121 <br /> 2,4-Dinitrotoluene U 1.39 48.6 146 03/25/202100:58 WG1639121 <br /> 2,6-Dinitrotoluene U 1.59 48.6 146 03/25/202100:58 WG1639121 <br /> Fluoranthene U 0.877 4.86 146 03/25/202100:58 WG1639121 <br /> Fluorene U 0.791 4.86 146 03/25/202100:58 WG1639121 <br /> Hexachlorobenzene U 1.72 48.6 146 03/25/202100:58 WG1639121 <br /> Hexachloro-1,3-butadiene U 1.64 48.6 146 03/25/202100:58 WG1639121 <br /> Hexachlorocyclopentadiene U 2.56 48.6 146 03/25/202100:58 WG1639121 <br /> Hexachloroethane U 1.91 48.6 146 03/25/202100:58 WG1639121 <br /> Indeno(1,2,3-cd)pyrene U 1.37 4.86 146 03/25/202100:58 WG1639121 <br /> Isophorone U 1.49 48.6 146 03/25/202100:58 WG1639121 <br /> Naphthalene 4.44 J 1.22 4.86 146 03/25/202100:58 WG1639121 <br /> Nitrobenzene U 1.69 48.6 146 03/25/202100:58 WG1639121 <br /> n-Nitrosodimethyla mine U 7.21 48.6 146 03/25/202100:58 WG1639121 <br /> n-Nitrosodiphenyla mine U 3.68 48.6 146 03/25/202100:58 WG1639121 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 7 of 32 <br />