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WG1638308 QUALITY CONTROL SUMMARY <br /> Volatile Organic Compounds (GC/MS) by Method 82608 L1328467-01 <br /> Method Blank (MB) FP1(MB)R3634237-3 03/21/2122:34 <br /> MB Result MB Qualifier MB MDL MB RDL <br /> FC Analyte mg/kg mg/kg mg/kg <br /> p-Isopropyltoluene U 0.00255 0.00500 <br /> 2-Butanone(MEK) 0.0711 J 0.0635 0.100 FSS <br /> Methylene Chloride U 0.00664 0.0250 <br /> 4-Methyl-2-pentanone(MIBK) U 0.00228 0.0250 rCn Methyl tert-butyl ether U 0.000350 0.00100 <br /> Naphthalene U 0.00488 0.0125 <br /> n-Propylbenzene U 0.000950 0.00500 FSr <br /> Styrene U 0.000229 0.0125 <br /> 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 <br /> 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 <br /> Tetrachloroethene U 0.000896 0.00250 <br /> Toluene U 0.00130 0.00500 7G1 <br /> 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 <br /> 1,2,3-Trichlorobe nzene U 0.00733 0.0125 <br /> 1,2,4-Trichlorobenzene U 0.00440 0.0125 FAI <br /> 1,1,1-Trichloroethane U 0.000923 0.00250 <br /> 1,1,2-Trichloroethane U 0.000597 0.00250 FSC <br /> Trichloroethene U 0.000584 0.00100 <br /> Trichlorofluoromethane U 0.000827 0.00250 <br /> 1,2,3-Trichloropropane U 0.00162 0.0125 <br /> 1,2,3-Trim ethyl benzene U 0.00158 0.00500 <br /> 1,2,4-Trimethylbenzene U 0.00158 0.00500 <br /> 1,3,5-Trim ethyl benzene U 0.00200 0.00500 <br /> Vinyl chloride U 0.00116 0.00250 <br /> Xylenes,Total U 0.000880 0.00650 <br /> (S)Toluene-d8 111 75.0-131 <br /> (S)4-Bromofluorobenzene 90.1 67.0-138 <br /> (S)1,2-Dich/oroethone-d4 83.9 70.0-130 <br /> Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) <br /> (LCS)R3634237-1 03/21/2121:18•(LCSD)R3634237-2 03/21/2121:37 <br /> Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits <br /> Analyte mg/kg mg/kg mg/kg % % % % % <br /> Acetone 0.625 0.949 1.33 152 213 10.0-160 J3 J4 33.4 31 <br /> Acrylonitrile 0.625 0.644 0.866 103 139 45.0-153 J3 29.4 22 <br /> Benzene 0.125 0.105 0.0986 84.0 78.9 70.0-123 6.29 20 <br /> Bromobenzene 0.125 0.121 0.115 96.8 92.0 73.0-121 5.08 20 <br /> Bromodichloromethane 0.125 0.105 0.105 84.0 84.0 73.0-121 0.000 20 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 17 of 32 <br />