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WG1638308 QUALITY CONTROL SUMMARY <br /> Volatile Organic Compounds (GC/MS) by Method 82608 L1328467-01 <br /> Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) <br /> FP1(LCS)R3634237-1 03/21/21 21:18•(LCSD)R3634237-2 03/21/2121:37 <br /> Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits FC Analyte mg/kg mg/kg mg/kg % % % % % <br /> Bromoform 0.125 0.133 0.133 106 106 64.0-132 0.000 20 <br /> Bromomethane 0.125 0.120 0.113 96.0 90.4 56.0-147 6.01 20 FSS <br /> n-Butylbenzene 0.125 0.102 0.103 81.6 82.4 68.0-135 0.976 20 <br /> sec-Butyl benzene 0.125 0.114 0.111 91.2 88.8 74.0-130 2.67 20 rCn tert-Butylbenzene 0.125 0.109 0.104 87.2 83.2 75.0-127 4.69 20 <br /> Carbon tetrachloride 0.125 0.109 0.101 87.2 80.8 66.0-128 7.62 20 <br /> Chlorobenzene 0.125 0.117 0.114 93.6 91.2 76.0-128 2.60 20 FSr <br /> Chlorodibromomethane 0.125 0.123 0.122 98.4 97.6 74.0-127 0.816 20 <br /> Chloroethane 0.125 0.107 0.107 85.6 85.6 61.0-134 0.000 20 <br /> Chloroform 0.125 0.106 0.103 84.8 82.4 72.0-123 2.87 20 <br /> Chloromethane 0.125 0.110 0.105 88.0 84.0 51.0-138 4.65 20 <br /> 2-Chlorotoluene 0.125 0.119 0.112 95.2 89.6 75.0-124 6.06 20 7G1 <br /> 4-Chlorotoluene 0.125 0.116 0.109 92.8 87.2 75.0-124 6.22 20 <br /> 1,2-Dibromo-3-Chloropropane 0.125 0.113 0.125 90.4 100 59.0-130 10.1 20 FAI 1,2-Dibromoethane 0.125 0.121 0.120 96.8 96.0 74.0-128 0.830 20 <br /> Dibromomethane 0.125 0.103 0.111 82.4 88.8 75.0-122 7.48 20 <br /> 1,2-Dichlorobenzene 0.125 0.115 0.115 92.0 92.0 76.0-124 0.000 20 FSC <br /> 1,3-Dichlorobenzene 0.125 0.117 0.114 93.6 91.2 76.0-125 2.60 20 <br /> 1,4-Dichlorobenzene 0.125 0.113 0.111 90.4 88.8 77.0-121 1.79 20 <br /> Dichlorodifluoromethane 0.125 0.105 0.104 84.0 83.2 43.0-156 0.957 20 <br /> 1,1-Dichloroethane 0.125 0.111 0.107 88.8 85.6 70.0-127 3.67 20 <br /> 1,2-Dichloroethane 0.125 0.109 0.105 87.2 84.0 65.0-131 3.74 20 <br /> 1,1-Dichloroethene 0.125 0.114 0.107 91.2 85.6 65.0-131 6.33 20 <br /> cis-1,2-Dichloroethene 0.125 0.106 0.101 84.8 80.8 73.0-125 4.83 20 <br /> trans-1,2-Dichloroethene 0.125 0.109 0.106 87.2 84.8 71.0-125 2.79 20 <br /> 1,2-Dichloropropane 0.125 0.116 0.114 92.8 91.2 74.0-125 1.74 20 <br /> 1,1-Dichloropropene 0.125 0.107 0.104 85.6 83.2 73.0-125 2.84 20 <br /> 1,3-Dichloropropane 0.125 0.115 0.113 92.0 90.4 80.0-125 1.75 20 <br /> cis-1,3-Dichloropropene 0.125 0.105 0.102 84.0 81.6 76.0-127 2.90 20 <br /> trans-1,3-Dichloropropene 0.125 0.121 0.118 96.8 94.4 73.0-127 2.51 20 <br /> 2,2-Dichloropropane 0.125 0.128 0.115 102 92.0 59.0-135 10.7 20 <br /> Di-isopropyl ether 0.125 0.109 0.107 87.2 85.6 60.0-136 1.85 20 <br /> Ethylbenzene 0.125 0.116 0.113 92.8 90.4 74.0-126 2.62 20 <br /> Hexachloro-1,3-butadiene 0.125 0.0962 0.102 77.0 81.6 57.0-150 5.85 20 <br /> Isopropylbenzene 0.125 0.111 0.108 88.8 86.4 72.0-127 2.74 20 <br /> p-Isopropyltoluene 0.125 0.109 0.107 87.2 85.6 72.0-133 1.85 20 <br /> 2-Butanone(MEK) 0.625 0.705 0.860 113 138 30.0-160 19.8 24 <br /> Methylene Chloride 0.125 0.114 0.109 91.2 87.2 68.0-123 4.48 20 <br /> 4-Methyl-2-pentanone(MIBK) 0.625 0.671 0.704 107 113 56.0-143 4.80 20 <br /> Methyl tert-butyl ether 0.125 0.0962 0.0958 77.0 76.6 66.0-132 0.417 20 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 18 of 32 <br />