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WG1638308 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260B L1328467-01 L1328914-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1(OS)L1328914-09 03/22/2104:02•(MS)R3634237-4 03/22/2107:12•(MSD)R3634237-5 03/22/2107:31 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits z Analyte mg/kg mg/kg mg/kg mg/kg % % % % % TC Carbon tetrachloride 0.103 U 0.0919 0.0898 89.2 87.2 1 10.0-145 2.31 37 Chlorobenzene 0.103 U 0.0993 0.0945 96.4 91.7 1 10.0-152 4.95 39 FSS Chlorodibromomethane 0.103 U 0.0984 0.0915 95.5 88.8 1 10.0-146 7.27 37 Chloroethane 0.103 U 0.0562 0.0446 54.6 43.3 1 10.0-146 23.0 40 rCn Chloroform 0.103 U 0.0885 0.0825 85.9 80.1 1 10.0-146 7.02 37 Chloromethane 0.103 U 0.0926 0.0960 89.9 93.2 1 10.0-159 3.61 37 2-Chlorotoluene 0.103 U 0.102 0.106 99.0 103 1 10.0-159 3.85 38 FSr 4-Chlorotoluene 0.103 U 0.101 0.106 98.1 103 1 10.0-155 4.83 39 1,2-Dibromo-3-Chloropropane 0.103 U 0.0824 0.0886 80.0 86.0 1 10.0-151 7.25 39 1,2-Dibromoethane 0.103 U 0.0980 0.0886 95.1 86.0 1 10.0-148 10.1 34 Dibromomethane 0.103 U 0.0733 0.0723 71.2 70.2 1 10.0-147 1.37 35 1,2-Dichlorobenzene 0.103 U 0.0919 0.0921 89.2 89.4 1 10.0-155 0.217 37 7G1 1,3-Dichlorobenzene 0.103 U 0.0938 0.0969 91.1 94.1 1 10.0-153 3.25 38 1,4-Dichlorobenzene 0.103 U 0.0941 0.0931 91.4 90.4 1 10.0-151 1.07 38 Dichlorodifluoromethane 0.103 U 0.0904 0.0945 87.8 91.7 1 10.0-160 4.43 35 FAI 1,1-Dichloroethane 0.103 U 0.0943 0.0896 91.6 87.0 1 10.0-147 5.11 37 1,2-Dichloroethane 0.103 U 0.0794 0.0694 77.1 67.4 1 10.0-148 13.4 35 [Sc 1,1-Dichloroethene 0.103 U 0.0974 0.0973 94.6 94.5 1 10.0-155 0.103 37 cis-1,2-Dichloroethene 0.103 U 0.0837 0.0794 81.3 77.1 1 10.0-149 5.27 37 trans-1,2-Dichloroethene 0.103 U 0.0857 0.0855 83.2 83.0 1 10.0-150 0.234 37 1,2-Dichloropropane 0.103 U 0.0938 0.0899 91.1 87.3 1 10.0-148 4.25 37 1,1-Dichloropropene 0.103 U 0.0923 0.0903 89.6 87.7 1 10.0-153 2.19 35 1,3-Dichloropropane 0.103 U 0.0977 0.0918 94.9 89.1 1 10.0-154 6.23 35 cis-1,3-Dichloropropene 0.103 U 0.0831 0.0791 80.7 76.8 1 10.0-151 4.93 37 trans-1,3-Dichloropropene 0.103 U 0.101 0.0966 98.1 93.8 1 10.0-148 4.45 37 2,2-Dichloropropane 0.103 U 0.0794 0.0742 77.1 72.0 1 10.0-138 6.77 36 Di-isopropyl ether 0.103 U 0.0951 0.0873 92.3 84.8 1 10.0-147 8.55 36 Ethylbenzene 0.103 U 0.0973 0.0971 94.5 94.3 1 10.0-160 0.206 38 Hexachloro-1,3-butadiene 0.103 U 0.0740 0.0858 71.8 83.3 1 10.0-160 14.8 40 Isopropylbenzene 0.103 U 0.0915 0.0890 88.8 86.4 1 10.0-155 2.77 38 p-Isopropyltoluene 0.103 U 0.0967 0.100 93.9 97.1 1 10.0-160 3.36 40 2-Butanone(MEK) 0.513 U 0.595 0.494 116 96.3 1 10.0-160 18.5 40 Methylene Chloride 0.103 U 0.0944 0.0285 91.7 27.7 1 10.0-141 J3 107 37 4-Methyl-2-pentanone(MIBK) 0.513 U 0.561 0.524 109 102 1 10.0-160 6.82 35 Methyl tert-butyl ether 0.103 U 0.0721 0.0637 70.0 61.8 1 11.0-147 12.4 35 Naphthalene 0.103 U 0.0631 0.0659 61.3 64.0 1 10.0-160 4.34 36 n-Propylbenzene 0.103 U 0.106 0.115 103 112 1 10.0-158 8.14 38 Styrene 0.103 U 0.0880 0.0838 85.4 81.4 1 10.0-160 4.89 40 1,1,1,2-Tetrachloroethane 0.103 U 0.0915 0.0826 88.8 80.2 1 10.0-149 10.2 39 1,1,2,2-Tetrachloroethane 0.103 U 0.109 0.111 106 108 1 10.0-160 1.82 35 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 20 of 32