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WG1638308 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 82606 L1328467-01 L1328914-09 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1(OS)L1328914-09 03/22/2104:02•(MS)R3634237-4 03/22/2107:12•(MSD)R3634237-5 03/22/2107:31 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits z Analyte mg/kg mg/kg mg/kg mg/kg % % % % % TC Tetrachloroethene 0.103 U 0.106 0.101 103 98.1 1 10.0-156 4.83 39 Toluene 0.103 U 0.103 0.0995 100 96.6 1 10.0-156 3.46 38 FSS 1,1,2-Trichlorotrifluoroethane 0.103 U 0.105 0.106 102 103 1 10.0-160 0.948 36 1,2,3-Trichlorobe nzene 0.103 U 0.0616 0.0661 59.8 64.2 1 10.0-160 7.05 40 rCn 1,2,4-Trichlorobenzene 0.103 U 0.0682 0.0679 66.2 65.9 1 10.0-160 0.441 40 1,1,1-Trichloroethane 0.103 U 0.0870 0.0795 84.5 77.2 1 10.0-144 9.01 35 1,1,2-Trichloroethane 0.103 U 0.0992 0.0928 96.3 90.1 1 10.0-160 6.67 35 FSr Trichloroethene 0.103 U 0.0879 0.0868 85.3 84.3 1 10.0-156 1.26 38 Trichlorofluoromethane 0.103 U 0.0683 0.0571 66.3 55.4 1 10.0-160 17.9 40 1,2,3-Trichloropropane 0.103 U 0.115 0.112 112 109 1 10.0-156 2.64 35 1,2,3-Trim ethyl benzene 0.103 U 0.0931 0.0936 90.4 90.9 1 10.0-160 0.536 36 1,2,4-Trimethylbenzene 0.103 U 0.0965 0.0950 93.7 92.2 1 10.0-160 1.57 36 7G1 1,3,5-Trim ethyl benzene 0.103 U 0.0995 0.103 96.6 100 1 10.0-160 3.46 38 Vinyl chloride 0.103 U 0.0887 0.0932 86.1 90.5 1 10.0-160 4.95 37 FAI Xylenes,Total 0.308 U 0.286 0.275 92.9 89.3 1 10.0-160 3.92 38 (S)Toluene-d8 112 111 75.0-131 (S)4-Bromofluorobenzene 90.9 89.3 67.0-138 (S)1,2-Dich/oroethane-d4 98.6 89.4 70.0-130 [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 21 of 32