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WG1639121 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1328467-01 Laboratory Control Sample (LCS) FP1(LCS)R3634595-1 03/24/2117:20 Spike Amount LCS Result LCS Rec. Rec.Limits LCS Qualifier z Analyte mg/kg mg/kg % % TC 2,4-Dinitrophenol 0.666 0.170 25.5 10.0-120 2-Nitrophenol 0.666 0.350 52.6 20.0-120 FSS 4-Nitrophenol 0.666 0.425 63.8 27.0-120 Pentachlorophenol 0.666 0.401 60.2 29.0-120 rCn Phenol 0.666 0.328 49.2 28.0-120 2,4,5-Trichlorophenol 0.666 0.370 55.6 38.0-120 2,4,6-Trichlorophenol 0.666 0.427 64.1 37.0-120 FSr (S)Nitrobenzene-d5 44.4 10.0-122 (S)2-Fluorobiphenyl 62.2 15.0-120 (S)p-Terphenyl-d14 67.6 10.0-120 (S)Phenol-d5 51.5 10.0-120 (S)2-F/uorophenol 57.8 12.0-120 G (S)2,4,6-Tribromopheno/ 73.6 10.0-127 rAl L1328413-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS)L1328413-07 03/24/2120:28•(MS)R3634595-3 03/24/2120:49•(MSD)R3634595-4 03/24/2121:10 [ScSpike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Acenaphthene 0.666 U 0.306 0.310 45.9 46.5 1 18.0-120 1.30 32 Acenaphthylene 0.666 U 0.322 0.325 48.3 48.8 1 25.0-120 0.927 32 Anthracene 0.666 U 0.347 0.353 52.1 53.0 1 22.0-120 1.71 29 Benzidine 1.33 U U U 0.000 0.000 1 10.0-120 J6 J6 0.000 40 Benzo(a)anthracene 0.666 U 0.378 0.391 56.8 58.7 1 25.0-120 3.38 29 Benzo(b)fluoranthene 0.666 U 0.415 0.436 62.3 65.5 1 19.0-122 4.94 31 Benzo(k)fluoranthene 0.666 U 0.408 0.432 61.3 64.9 1 23.0-120 5.71 30 Benzo(g,h,i)perylene 0.666 U 0.286 0.285 42.9 42.8 1 10.0-120 0.350 33 Benzo(a)pyrene 0.666 U 0.417 0.434 62.6 65.2 1 24.0-120 4.00 30 Bis(2-chlorethoxy)methane 0.666 U 0.241 0.237 36.2 35.6 1 10.0-120 1.67 34 Bis(2-chloroethyl)ether 0.666 U 0.380 0.363 57.1 54.5 1 10.0-120 4.58 40 2,2-Oxybis(1-Chloropropane) 0.666 U 0.278 0.257 41.7 38.6 1 10.0-120 7.85 40 4-Bromophenyl-phenylether 0.666 U 0.407 0.412 61.1 61.9 1 27.0-120 1.22 30 2-Chloronaphthalene 0.666 U 0.330 0.323 49.5 48.5 1 20.0-120 2.14 32 4-Chlorophenyl-phenylether 0.666 U 0.382 0.395 57.4 59.3 1 24.0-120 3.35 29 Chrysene 0.666 U 0.372 0.388 55.9 58.3 1 21.0-120 4.21 29 Dibenz(a,h)anthracene 0.666 U 0.299 0.301 44.9 45.2 1 10.0-120 0.667 32 3,3-Dichlorobenzidine 1.33 U 0.276 0.188 20.8 14.1 1 10.0-120 J3 37.9 34 2,4-Dinitrotoluene 0.666 U 0.406 0.419 61.0 62.9 1 30.0-120 3.15 31 2,6-Dinitrotoluene 0.666 U 0.363 0.382 54.5 57.4 1 25.0-120 5.10 31 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 26 of 32