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WG1639121 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270C L1328467-01 L1328413-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) FP1(OS)L1328413-07 03/24/2120:28•(MS)R3634595-3 03/24/2120:49•(MSD)R3634595-4 03/24/2121:10 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits 17c Analyte mg/kg mg/kg mg/kg mg/kg % % % % % Fluoranthene 0.666 U 0.381 0.390 57.2 58.6 1 18.0-126 2.33 32 Fluorene 0.666 U 0.348 0.358 52.3 53.8 1 25.0-120 2.83 30 FSS Hexachlorobenzene 0.666 U 0.401 0.400 60.2 60.1 1 27.0-120 0.250 28 Hexachloro-1,3-butadiene 0.666 U 0.321 0.310 48.2 46.5 1 10.0-120 3.49 38 rCn Hexachlorocyclopentadiene 0.666 U 0.276 0.269 41.4 40.4 1 10.0-120 2.57 40 Hexachloroethane 0.666 U 0.259 0.237 38.9 35.6 1 10.0-120 8.87 40 Indeno(1,2,3-cd)pyrene 0.666 U 0.307 0.306 46.1 45.9 1 10.0-120 0.326 32 FSr Isophorone 0.666 U 0.232 0.226 34.8 33.9 1 13.0-120 2.62 34 Naphthalene 0.666 U 0.269 0.255 40.4 38.3 1 10.0-120 5.34 35 Nitrobenzene 0.666 U 0.222 0.208 33.3 31.2 1 10.0-120 6.51 36 n-Nitrosodimethyla mine 0.666 U 0.165 0.153 24.8 23.0 1 10.0-127 7.55 40 n-Nitrosodiphenyla mine 0.666 U 0.324 0.325 48.6 48.8 1 17.0-120 0.308 29 7G1 n-Nitrosodi-n-propylamine 0.666 U 0.239 0.230 35.9 34.5 1 10.0-120 3.84 37 Phenanthrene 0.666 U 0.358 0.369 53.8 55.4 1 17.0-120 3.03 31 Benzylbutyl phthalate 0.666 U 0.376 0.391 56.5 58.7 1 23.0-120 3.91 30 FAI Bis(2-ethylhexyl)phthalate 0.666 U 0.341 0.356 51.2 53.5 1 17.0-126 4.30 30 Di-n-butyl phthalate 0.666 U 0.353 0.360 53.0 54.1 1 30.0-120 1.96 29 FSC Diethyl phthalate 0.666 U 0.366 0.380 55.0 57.1 1 26.0-120 3.75 28 Dimethyl phthalate 0.666 U 0.352 0.366 52.9 55.0 1 25.0-120 3.90 29 Di-n-octyl phthalate 0.666 U 0.311 0.324 46.7 48.6 1 21.0-123 4.09 29 Pyrene 0.666 U 0.400 0.418 60.1 62.8 1 16.0-121 4.40 32 Pyridine 0.666 U 0.0670 0.0574 10.1 8.62 1 10.0-120 J6 15.4 40 1,2,4-Trichlorobenzene 0.666 U 0.311 0.287 46.7 43.1 1 12.0-120 8.03 37 4-Chloro-3-methylphenol 0.666 U 0.266 0.281 39.9 42.2 1 15.0-120 5.48 30 2-Chlorophenol 0.666 U 0.308 0.299 46.2 44.9 1 15.0-120 2.97 37 2-Methylphenol 0.666 U 0.409 0.401 61.4 60.2 1 11.0-120 1.98 40 3&4-Methyl Phenol 0.666 U 0.333 0.333 50.0 50.0 1 12.0-123 0.000 38 2,4-Dichlorophenol 0.666 U 0.325 0.325 48.8 48.8 1 20.0-120 0.000 31 2,4-Dimethylphenol 0.666 U 0.261 0.258 39.2 38.7 1 10.0-120 1.16 33 4,6-Dinitro-2-methylphenol 0.666 U 0.386 0.392 58.0 58.9 1 10.0-120 1.54 39 2,4-Dinitrophenol 0.666 U 0.340 0.344 51.1 51.7 1 10.0-121 1.17 40 2-Nitrophenol 0.666 U 0.304 0.288 45.6 43.2 1 12.0-120 5.41 39 4-Nitrophenol 0.666 U 0.377 0.381 56.6 57.2 1 10.0-137 1.06 32 Pentachlorophenol 0.666 U 0.427 0.441 64.1 66.2 1 10.0-160 3.23 31 Phenol 0.666 U 0.262 0.259 39.3 38.9 1 12.0-120 1.15 38 2,4,5-Trichlorophenol 0.666 U 0.326 0.349 48.9 52.4 1 20.0-120 6.81 30 2,4,6-Trichlorophenol 0.666 U 0.350 0.362 52.6 54.4 1 19.0-120 3.37 32 (S)Nitrobenzene-d5 35.7 33.9 10.0-122 (S)2-F/uorobiphenyl 51.4 50.8 15.0-120 (S)p-Terphenyl-d14 58.9 62.2 10.0-120 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc 79023 L1328467 03/26/2111:37 27 of 32