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DRUMS OILY SLUDGE #4 SAMPLE RESULTS - 04 Collected date/time: 08/11/21 07:00 L1391519 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/kg mg/kg mg/kg date/time Bromodichloromethane U 0.00293 0.0101 4.04 08/23/202116:32 WG1727785 FTc Bromoform U 0.00473 0.101 4.04 08/23/202116:32 WG1727785 Bromomethane U 0.00796 0.0505 4.04 08/23/202116:32 WG1727785 FSS n-Butylbenzene 0.103 0.0212 0.0505 4.04 08/23/202116:32 WG1727785 sec-Butyl benzene 0.0264 J 0.0116 0.0505 4.04 08/23/202116:32 WG1727785 tert-Butylbenzene U 0.00788 0.0202 4.04 08/23/202116:32 WG1727785 4 Cn Carbon tetrachloride U 0.00363 0.0202 4.04 08/23/202116:32 WG1727785 Chlorobenzene U 0.000848 0.0101 4.04 08/23/202116:32 WG1727785 Chlorodibromomethane U 0.00247 0.0101 4.04 08/23/202116:32 WG1727785 Chloroethane U 0.00687 0.0202 4.04 08/23/202116:32 WG1727785 Chloroform U 0.00416 0.0101 4.04 08/23/202116:32 WG1727785 RC Chloromethane U 0.0176 0.0505 4.04 08/23/202116:32 WG1727785 2-Chlorotoluene U 0.00349 0.0101 4.04 08/23/202116:32 WG1727785 4-Chlorotoluene U 0.00182 0.0202 4.04 08/23/202116:32 WG1727785 GI 1,2-Dibromo-3-Chloropropane U 0.0158 0.101 4.04 08/23/202116:32 WG1727785 1,2-Dibromoethane U 0.00262 0.0101 4.04 08/23/202116:32 WG1727785 FAI Dibromomethane U 0.00303 0.0202 4.04 08/23/202116:32 WG1727785 1,2-Dichlorobenzene U 0.00172 0.0202 4.04 08/23/202116:32 WG1727785 FSC 1,3-Dichlorobenzene U 0.00242 0.0202 4.04 08/23/202116:32 WG1727785 1,4-Dichlorobenzene U 0.00283 0.0202 4.04 08/23/202116:32 WG1727785 Dichlorodifluoromethane U 0.00650 0.0101 4.04 08/23/202116:32 WG1727785 1,1-Dichloroethane U 0.00198 0.0101 4.04 08/23/202116:32 WG1727785 1,2-Dichloroethane U 0.00262 0.0101 4.04 08/23/202116:32 WG1727785 1,1-Dichloroethene U 0.00245 0.0101 4.04 08/23/202116:32 WG1727785 cis-1,2-Dichloroethene U 0.00297 0.0101 4.04 08/23/202116:32 WG1727785 trans-1,2-Dichloroethene U 0.00420 0.0202 4.04 08/23/202116:32 WG1727785 1,2-Dichloropropane U 0.00574 0.0202 4.04 08/23/202116:32 WG1727785 1,1-Dichloropropene U 0.00327 0.0101 4.04 08/23/202116:32 WG1727785 1,3-Dichloropropane U 0.00202 0.0202 4.04 08/23/202116:32 WG1727785 cis-1,3-Dichloropropene U 0.00306 0.0101 4.04 08/23/202116:32 WG1727785 trans-1,3-Dichloropropene U 0.00461 0.0202 4.04 08/23/202116:32 WG1727785 2,2-Dichloropropane U 0.00558 0.0101 4.04 08/23/202116:32 WG1727785 Di-isopropyl ether U 0.00166 0.00404 4.04 08/23/202116:32 WG1727785 Ethylbenzene 0.0267 0.00298 0.0101 4.04 08/23/202116:32 WG1727785 Hexachloro-1,3-butadiene U 0.0242 0.101 4.04 08/23/202116:32 WG1727785 Isopropylbenzene U 0.00172 0.0101 4.04 08/23/202116:32 WG1727785 p-Isopropyltoluene 0.0229 0.0103 0.0202 4.04 08/23/202116:32 WG1727785 2-Butanone(MEK) 0.527 B J4 0.257 0.404 4.04 08/23/202116:32 WG1727785 Methylene Chloride U 0.0268 0.101 4.04 08/23/202116:32 WG1727785 4-Methyl-2-pentanone(MIBK) 0.931 0.00921 0.101 4.04 08/23/202116:32 WG1727785 Methyl tert-butyl ether U 0.00141 0.00404 4.04 08/23/202116:32 WG1727785 Naphthalene 0.722 0.0197 0.0505 4.04 08/23/202116:32 WG1727785 n-Propylbenzene 0.0392 0.00384 0.0202 4.04 08/23/202116:32 WG1727785 Styrene U 0.000925 0.0505 4.04 08/23/202116:32 WG1727785 1,1,1,2-Tetrachloroethane U 0.00383 0.0101 4.04 08/23/202116:32 WG1727785 1,1,2,2-Tetrachloroethane U 0.00281 0.0101 4.04 08/23/202116:32 WG1727785 1,1,2-Trichlorotrifluoroethane U 0.00305 0.0101 4.04 08/23/202116:32 WG1727785 Tetrachloroethene 0.124 0.00362 0.0101 4.04 08/23/202116:32 WG1727785 Toluene 0.0436 0.00525 0.0202 4.04 08/23/202116:32 WG1727785 1,2,3-Trichlorobenzene U 0.0296 0.0505 4.04 08/23/202116:32 WG1727785 1,2,4-Trichlorobenzene U 0.0178 0.0505 4.04 08/23/202116:32 WG1727785 1,1,1-Trichloroethane U 0.00373 0.0101 4.04 08/23/202116:32 WG1727785 1,1,2-Trichloroethane U 0.00241 0.0101 4.04 08/23/202116:32 WG1727785 Trichloroethene U 0.00236 0.00404 4.04 08/23/202116:32 WG1727785 Trichlorofluoromethane U 0.00334 0.0101 4.04 08/23/202116:32 WG1727785 1,2,3-Trichloropropane U 0.00654 0.0505 4.04 08/23/202116:32 WG1727785 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc AIS 81046-16 L1391519 08/27/2109:46 18 of 44